4-Chloro-N-cyclohexylbenzamide

Base Information

• Chemical Name: 4-Chloro-N-cyclohexylbenzamide
• CAS No.: 57707-20-7
• Molecular Formula: C13H16ClNO
• Molecular Weight: 237.729
• Hs Code.: 2924299090
• Mol file: 57707-20-7.mol

Synonyms:4-Chloro-N-cyclohexylbenzamide;N-Cyclohexyl-4-chlorobenzamide;N-Cyclohexyl-p-chlorobenzamide;NSC 14855;

Chemical Property of 4-Chloro-N-cyclohexylbenzamide

Chemical Property:

• Vapor Pressure: 1.82E-06mmHg at 25°C
• Refractive Index: 1.561
• Boiling Point: 395.6 °C at 760 mmHg
• Flash Point: 193 °C
• PSA: 29.10000
• Density: 1.17 g/cm³
• LogP: 3.79340

Purity/Quality:

97% ^*data from raw suppliers

N-Cyclohexyl4-Chlorobenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Chloro-N-cyclohexylbenzamide

There total 32 articles about 4-Chloro-N-cyclohexylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

cyclohexylamine (108-91-8,157973-60-9) + para-chlorobenzoic acid (74-11-3) → 4-chloro-N-cyclohexylbenzamide (57707-20-7)

Guidance literature:

para-chlorobenzoic acid; With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate; triphenylphosphine; at 20 ℃; for 0.166667h;

cyclohexylamine; at 20 ℃; for 0.333333h;

DOI:10.1039/c5ra10127a

Reference yield: 96.0%

cyclohexane (110-82-7,25012-93-5) + 4-chlorobenzamide (619-56-7) → 4-chloro-N-cyclohexylbenzamide (57707-20-7)

Guidance literature:

With copper acetylacetonate; di-tert-butyl peroxide; at 115 ℃; for 12h; Sealed tube; Schlenk technique;

DOI:10.1039/c5cc00839e

Reference yield: 95.0%

C13H16ClNO (23898-55-7) → 4-chloro-N-cyclohexylbenzamide (57707-20-7)

Guidance literature:

With iron(III) sulfate pentahydrate; sodium dodecyl-sulfate; In water; at 20 - 70 ℃; for 1.66667h; Green chemistry;

DOI:10.1039/c6gc03589b

upstream raw materials:

Cyclohexyl isocyanide

2-Amino-4-chlorobenzoic acid

cyclohexylamine

1-Chloro-4-iodobenzene

Downstream raw materials:

N-cyclohexyl 4-chlorobenzimidoyl chloride

C₁₉H₂₀ClN₃O

2-chloro-N-(4-nitrophenyl)benzamide

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