Technology Process of C47H70N8O10
There total 12 articles about C47H70N8O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
methanol;
for 24h;
under 760.051 Torr;
DOI:10.1021/jm301630s
- Guidance literature:
-
Multi-step reaction with 7 steps
1: hydrogen; palladium on activated charcoal / ethyl acetate / 2 h / 760.05 Torr
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / tetrahydrofuran
3: hydrogen; palladium on activated charcoal / ethyl acetate / 2 h / 760.05 Torr
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C
5: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
6: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 26 h / 0 - 20 °C
7: hydrogen; palladium on activated charcoal / methanol / 24 h / 760.05 Torr
With
1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm301630s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C
2: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
3: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 26 h / 0 - 20 °C
4: hydrogen; palladium on activated charcoal / methanol / 24 h / 760.05 Torr
With
1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid;
In
methanol; dichloromethane;
DOI:10.1021/jm301630s