2-(2-Hydroxymethylphenyl)-acetaldehyddimethylacetal

Base Information

Chemical Name:2-(2-Hydroxymethylphenyl)-acetaldehyddimethylacetal
CAS No.:130089-24-6
Molecular Formula:C₁₁H₁₆O₃
Molecular Weight:196.246
Hs Code.:

Synonyms:2-(2-Hydroxymethylphenyl)-acetaldehyddimethylacetal

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Chemical Property of 2-(2-Hydroxymethylphenyl)-acetaldehyddimethylacetal

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Technology Process of 2-(2-Hydroxymethylphenyl)-acetaldehyddimethylacetal

There total 5 articles about 2-(2-Hydroxymethylphenyl)-acetaldehyddimethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.1%

: 112396-12-0
Homophthalaldehyd-monodimethylacetal

: 130089-24-6
2-(2-Hydroxymethylphenyl)-acetaldehyddimethylacetal

Guidance literature:: With sodium tetrahydroborate; In methanol; for 5h; Ambient temperature;
DOI:10.1002/ardp.19903230810

Reference yield:

: 130089-19-9,130089-23-5,59436-11-2
1-bromo-2-(2-methoxyethenyl)benzene

: 130089-24-6
2-(2-Hydroxymethylphenyl)-acetaldehyddimethylacetal

Guidance literature:: Multi-step reaction with 2 steps

1: 93.2 percent / p-TsOH / 65 h / Heating

2: 1.) n-BuLi / 1.) THF, hexane, 1 h, -78 deg C, 2.a) THF, 2 h, -78 deg C, 2.b) 2 h, room temperature

With n-butyllithium; toluene-4-sulfonic acid;
DOI:10.1002/ardp.19903230810

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 130089-24-6
2-(2-Hydroxymethylphenyl)-acetaldehyddimethylacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) K-tert.-butylat / 1.) THF, -10 deg C, 2.a) -10 deg C, 2.b) 16 h, room temperature

2: 93.2 percent / p-TsOH / 65 h / Heating

3: 1.) n-BuLi / 1.) THF, hexane, 1 h, -78 deg C, 2.a) THF, 2 h, -78 deg C, 2.b) 2 h, room temperature

With n-butyllithium; potassium tert-butylate; toluene-4-sulfonic acid;
DOI:10.1002/ardp.19903230810