[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Base Information

Chemical Name:[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester
CAS No.:936132-33-1
Molecular Formula:C₅₇H₆₁NO₁₃
Molecular Weight:968.11
Hs Code.:

Synonyms:[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Suppliers and Price of [2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

There total 4 articles about [2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 936132-31-9
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-6-O-(4-methoxybenzyl)-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

: 936132-33-1
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; for 26h;
DOI:10.1016/j.tet.2008.06.089

Reference yield:

: 913725-93-6
(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-(4-methoxy-benzyloxymethyl)-tetrahydro-pyran-2-carboxylic acid

: 936132-33-1
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / diphenyl phosphoryl azide; Et₃N / benzene / 4 h / Heating

2: 81 percent / DDQ; H₂O / CH₂Cl₂

With diphenyl phosphoryl azide; water; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; benzene; 1: Curtius rearrangement;
DOI:10.1002/ejoc.200600993

Reference yield:

: C₃₇H₄₀O₈

: 936132-33-1
[2,3,4-tri-O-benzyl-6-O-{(N-2,3,4-tris-O-benzyl-β-D-glucopyranosyl)carbamoyl}-β-D-glucopyranosyl]formic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / DDQ

2: 84 percent / diphenyl phosphoryl azide; Et₃N / benzene / 4 h / Heating

3: 81 percent / DDQ; H₂O / CH₂Cl₂

With diphenyl phosphoryl azide; water; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; benzene; 2: Curtius rearrangement;
DOI:10.1002/ejoc.200600993