phosphoric acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 3-hydroxy-5-(5-methyl-2,4-dioxo-5-phenylselanyl-tetrahydro-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

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Chemical Name:phosphoric acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 3-hydroxy-5-(5-methyl-2,4-dioxo-5-phenylselanyl-tetrahydro-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester
CAS No.:698345-07-2
Molecular Formula:C₄₆H₄₉N₄O₁₄PSe
Molecular Weight:991.847
Hs Code.:

phosphoric acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2<i>H</i>-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 3-hydroxy-5-(5-methyl-2,4-dioxo-5-phenylselanyl-tetrahydro-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

Synonyms:phosphoric acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 3-hydroxy-5-(5-methyl-2,4-dioxo-5-phenylselanyl-tetrahydro-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

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Chemical Property of phosphoric acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 3-hydroxy-5-(5-methyl-2,4-dioxo-5-phenylselanyl-tetrahydro-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

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Technology Process of phosphoric acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 3-hydroxy-5-(5-methyl-2,4-dioxo-5-phenylselanyl-tetrahydro-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

There total 5 articles about phosphoric acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 3-hydroxy-5-(5-methyl-2,4-dioxo-5-phenylselanyl-tetrahydro-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 349490-16-0
C₄₉H₅₂N₅O₁₄PSe

: 698345-07-2
phosphoric acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 3-hydroxy-5-(5-methyl-2,4-dioxo-5-phenylselanyl-tetrahydro-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; for 12h; Heating;
DOI:10.1021/ja010180s

Reference yield:

: 109389-30-2
Diisopropyl-phosphoramidous acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-cyano-ethyl ester

: 698345-07-2
phosphoric acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 3-hydroxy-5-(5-methyl-2,4-dioxo-5-phenylselanyl-tetrahydro-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrazole / acetonitrile; tetrahydrofuran / 4 h / 0 °C

1.2: 58 percent / I₂; 2,6-lutidine; H₂O / tetrahydrofuran

2.1: Et₃N / tetrahydrofuran / 12 h / Heating

With 1H-tetrazole; triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ja010180s

Reference yield:

: 208466-63-1
1-[(2R,4S,5R)-4-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-5-methyl-5-phenylselanyl-dihydro-pyrimidine-2,4-dione

: 698345-07-2
phosphoric acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 3-hydroxy-5-(5-methyl-2,4-dioxo-5-phenylselanyl-tetrahydro-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 0.081 g / TFA / tetrahydrofuran; H₂O / 4 h / 0 °C

2.1: 88 percent / Et₃N*3HF / tetrahydrofuran / 12 h

3.1: tetrazole / acetonitrile; tetrahydrofuran / 4 h / 0 °C

3.2: 58 percent / I₂; 2,6-lutidine; H₂O / tetrahydrofuran

4.1: Et₃N / tetrahydrofuran / 12 h / Heating

With 1H-tetrazole; triethylamine tris(hydrogen fluoride); triethylamine; trifluoroacetic acid; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/ja010180s