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Technology Process of [W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl](1+)*AlCl4(1-)=[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl]AlCl4

[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl](1+)*AlCl4(1-)=[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl]AlCl4

Base Information
  • Chemical Name:[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl](1+)*AlCl4(1-)=[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl]AlCl4
  • CAS No.:83634-35-9
  • Molecular Formula:AlCl4*C17H33ClNP2W
  • Molecular Weight:701.5
  • Hs Code.:
[W(NC<sub>6</sub>H<sub>5</sub>)(CHC(CH<sub>3</sub>)3)(P(CH<sub>3</sub>)3)2Cl]<sup>(1+)</sup>*AlCl<sub>4</sub><sup>(1-)</sup>=[W(NC<sub>6</sub>H<sub>5</sub>)(CHC(CH<sub>3</sub>)3)(P(CH<sub>3</sub>)3)2Cl]AlCl<sub>4</sub>

Synonyms:[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl](1+)*AlCl4(1-)=[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl]AlCl4

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Chemical Property of [W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl](1+)*AlCl4(1-)=[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl]AlCl4
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Technology Process of [W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl](1+)*AlCl4(1-)=[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl]AlCl4

There total 1 articles about [W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl](1+)*AlCl4(1-)=[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl]AlCl4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

aluminium trichloride
7446-70-0

aluminium trichloride

W(NC<sub>6</sub>H<sub>5</sub>)(CHC(CH<sub>3</sub>)3)(P(CH<sub>3</sub>)3)2Cl<sub>2</sub>
83634-33-7

W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl2

[W(NC<sub>6</sub>H<sub>5</sub>)(CHC(CH<sub>3</sub>)3)(P(CH<sub>3</sub>)3)2Cl]<sup>(1+)</sup>*AlCl<sub>4</sub><sup>(1-)</sup>=[W(NC<sub>6</sub>H<sub>5</sub>)(CHC(CH<sub>3</sub>)3)(P(CH<sub>3</sub>)3)2Cl]AlCl<sub>4</sub>
83634-35-9

[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl](1+)*AlCl4(1-)=[W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl]AlCl4

Guidance literature:
In dichloromethane; W complex dissolved in CH2Cl2 under N2, AlCl3 added, mixture stirred for 0.5 h; filtration through Celite, concg. in vac., cooling to -30°C; elem. anal.;
DOI:10.1021/ja00390a016
upstream raw materials:

aluminium trichloride

W(NC6H5)(CHC(CH3)3)(P(CH3)3)2Cl2

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