chloro(diphenyl-p-tolylphosphine)gold(I)

Base Information

Chemical Name:chloro(diphenyl-p-tolylphosphine)gold(I)
CAS No.:107198-68-5
Molecular Formula:C₁₉H₁₇AuClP
Molecular Weight:508.737
Hs Code.:

Synonyms:chloro(diphenyl-p-tolylphosphine)gold(I)

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Chemical Property of chloro(diphenyl-p-tolylphosphine)gold(I)

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Technology Process of chloro(diphenyl-p-tolylphosphine)gold(I)

There total 8 articles about chloro(diphenyl-p-tolylphosphine)gold(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 50960-82-2
carbonylgold(I) chloride

: 1031-93-2
diphenyl(p-tolyl)phosphine

: 107198-68-5
chloro(diphenyl-p-tolylphosphine)gold(I)

Guidance literature:: In diethyl ether; byproducts: CO; under N2; dropwise addn. of soln. of phosphane to suspension of Au-compd. at 0°C, stirred for 20 h; concd., pptn. by addn. of pentane; elem. anal.;

Reference yield:

: 75-54-7
Dichloromethylsilane

: 107198-69-6
Ph₂TolPAuCH₃

: 107198-68-5
chloro(diphenyl-p-tolylphosphine)gold(I)

: 7440-57-5,457905-15-6
gold

Guidance literature:: In tetrahydrofuran; dichloromethane; byproducts: HSiMe2Cl; To a soln. of Ph2TolPAuMe in CH2Cl2 or THF was added HSiMeCl2 and stirred some h at room temp., filtered (Au) and the volatile was removed in high vac.; washing with ether, crystn. with petroleum ether, washing with petroleum ether, drying in high vac.;

Reference yield:

: 107198-69-6
Ph₂TolPAuCH₃

: 1631-83-0
diphenylsilyl chloride

: 107198-68-5
chloro(diphenyl-p-tolylphosphine)gold(I)

: 7440-57-5,457905-15-6
gold

Guidance literature:: In tetrahydrofuran; dichloromethane; byproducts: HSiPh2Me; To a soln. of Ph2TolPAuMe in CH2Cl2 or THF was added HSiPh2Cl and stirred some h at room temp., filtered (Au) and the volatile was removed in high vac.; washing with ether, crystn. with petroleum ether, washing with petroleum ether, drying in high vac.;