methyl (S)-2-(isopropylamino)-3-(4-nitrophenyl)propanoate hydrochloride

Base Information

Chemical Name:methyl (S)-2-(isopropylamino)-3-(4-nitrophenyl)propanoate hydrochloride
CAS No.:1312680-08-2
Molecular Formula:C₁₃H₁₈N₂O₄*ClH
Molecular Weight:302.758
Hs Code.:

Synonyms:methyl (S)-2-(isopropylamino)-3-(4-nitrophenyl)propanoate hydrochloride

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Chemical Property of methyl (S)-2-(isopropylamino)-3-(4-nitrophenyl)propanoate hydrochloride

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Technology Process of methyl (S)-2-(isopropylamino)-3-(4-nitrophenyl)propanoate hydrochloride

There total 1 articles about methyl (S)-2-(isopropylamino)-3-(4-nitrophenyl)propanoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 17193-40-7
(S)-4-nitrophenylalanine methyl ester hydrochloride

: 67-64-1
acetone

: 1312680-08-2
methyl (S)-2-(isopropylamino)-3-(4-nitrophenyl)propanoate hydrochloride

Guidance literature:: With sodium tetrahydroborate; sodium acetate; acetic acid; In methanol; at 0 - 20 ℃; for 51h; chemoselective reaction;
DOI:10.1016/j.tetasy.2011.03.014

Reference yield:

: 1312680-08-2
methyl (S)-2-(isopropylamino)-3-(4-nitrophenyl)propanoate hydrochloride

: 79-04-9
chloroacetyl chloride

: C₁₅H₁₉ClN₂O₅

Guidance literature:: With 4-methyl-morpholine; In dichloromethane; at 0 - 20 ℃; for 1.75h;
DOI:10.1016/j.tetasy.2011.03.014

Reference yield:

: 1312680-08-2
methyl (S)-2-(isopropylamino)-3-(4-nitrophenyl)propanoate hydrochloride

: 1312680-10-6
(S)-1-isopropyl-6-(4-nitrobenzyl)piperazine-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine / dichloromethane / 1.75 h / 0 - 20 °C

2: ammonia / methanol / 24.5 h / 0 - 20 °C

With 4-methyl-morpholine; ammonia; In methanol; dichloromethane;
DOI:10.1016/j.tetasy.2011.03.014