Phosphoric acid dibenzyl ester (1R,2R,3S,4R,5R,6R)-2,3,6-tris-benzyloxy-5-(bis-benzyloxy-phosphanyloxy)-4-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Base Information

Chemical Name:Phosphoric acid dibenzyl ester (1R,2R,3S,4R,5R,6R)-2,3,6-tris-benzyloxy-5-(bis-benzyloxy-phosphanyloxy)-4-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester
CAS No.:162879-96-1
Molecular Formula:C₆₉H₆₉O₁₄P₃
Molecular Weight:1215.22
Hs Code.:

Phosphoric acid dibenzyl ester (1R,2R,3S,4R,5R,6R)-2,3,6-tris-benzyloxy-5-(bis-benzyloxy-phosphanyloxy)-4-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Synonyms:Phosphoric acid dibenzyl ester (1R,2R,3S,4R,5R,6R)-2,3,6-tris-benzyloxy-5-(bis-benzyloxy-phosphanyloxy)-4-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

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Chemical Property of Phosphoric acid dibenzyl ester (1R,2R,3S,4R,5R,6R)-2,3,6-tris-benzyloxy-5-(bis-benzyloxy-phosphanyloxy)-4-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

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Technology Process of Phosphoric acid dibenzyl ester (1R,2R,3S,4R,5R,6R)-2,3,6-tris-benzyloxy-5-(bis-benzyloxy-phosphanyloxy)-4-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

There total 9 articles about Phosphoric acid dibenzyl ester (1R,2R,3S,4R,5R,6R)-2,3,6-tris-benzyloxy-5-(bis-benzyloxy-phosphanyloxy)-4-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 145842-31-5
(+)-2,3,6-tri-O-benzyl-D-myo-inositol 1,4-O-bis(dibenzyl phosphate)

: 162879-96-1
Phosphoric acid dibenzyl ester (1R,2R,3S,4R,5R,6R)-2,3,6-tris-benzyloxy-5-(bis-benzyloxy-phosphanyloxy)-4-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Guidance literature:: DOI:10.1016/0008-6215(92)85046-3

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 162879-96-1
Phosphoric acid dibenzyl ester (1R,2R,3S,4R,5R,6R)-2,3,6-tris-benzyloxy-5-(bis-benzyloxy-phosphanyloxy)-4-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: tetrazole / CH₂Cl₂

2: 88 percent / 3-chloroperoxybenzoic acid

3: dichlorodicyanobenzoquinone / CH₂Cl₂; H₂O

With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;
DOI:10.1016/0008-6215(92)85046-3

Reference yield:

: 114218-16-5,114297-86-8,114419-07-7,145843-73-8
1D-(+)-1-O-allyl-2,3,6-tri-O-benzyl-myo-inositol

: 162879-96-1
Phosphoric acid dibenzyl ester (1R,2R,3S,4R,5R,6R)-2,3,6-tris-benzyloxy-5-(bis-benzyloxy-phosphanyloxy)-4-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 8 steps

2: potassium tert-butoxide / dimethylsulfoxide / 50 °C

3: NaH / dimethylformamide

4: 89 percent / 1M HCl / acetone; methanol / 0.67 h / 40 °C

5: tetrazole / CH₂Cl₂

6: 88 percent / 3-chloroperoxybenzoic acid

7: dichlorodicyanobenzoquinone / CH₂Cl₂; H₂O

With 1H-tetrazole; hydrogenchloride; potassium tert-butylate; sodium hydride; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0008-6215(92)85046-3