1-allylcyclohexanecarboxylic acid tert-butyl ester

Base Information

• Chemical Name: 1-allylcyclohexanecarboxylic acid tert-butyl ester
• CAS No.: 1001379-51-6
• Molecular Formula: C₁₄H₂₄O₂
• Molecular Weight: 224.343
• Mol file: 1001379-51-6.mol

Synonyms:1-allylcyclohexanecarboxylic acid tert-butyl ester

Chemical Property of 1-allylcyclohexanecarboxylic acid tert-butyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1-allylcyclohexanecarboxylic acid tert-butyl ester

There total 1 articles about 1-allylcyclohexanecarboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl cyclohexanecarboxylate (16537-05-6) + allyl bromide (106-95-6) → 1-allylcyclohexanecarboxylic acid tert-butyl ester (1001379-51-6)

Guidance literature:

tert-butyl cyclohexanecarboxylate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -20 - 0 ℃;

allyl bromide; In tetrahydrofuran; hexane; at -20 - 20 ℃; for 1.5h; Further stages.;

DOI:10.1021/jo701894v

Reference yield:

1-allylcyclohexanecarboxylic acid tert-butyl ester (1001379-51-6) → 1-(2-oxo-ethyl)cyclohexanecarboxylic acid tert-butyl ester (1001379-53-8)

Guidance literature:

1-allylcyclohexanecarboxylic acid tert-butyl ester; With ozone; In isopropyl alcohol; at -25 ℃; for 4h;

With sodium carbonate; phosphorous acid trimethyl ester; In isopropyl alcohol; at -15 ℃; for 1h; Further stages.;

DOI:10.1021/jo701894v

Reference yield:

methanol (67-56-1) + 1-allylcyclohexanecarboxylic acid tert-butyl ester (1001379-51-6) → 1-(2-oxo-ethyl)cyclohexanecarboxylic acid tert-butyl ester (1001379-53-8) + C15H28O4

Guidance literature:

methanol; 1-allylcyclohexanecarboxylic acid tert-butyl ester; With ozone;

With phosphorous acid trimethyl ester; Further stages.;

DOI:10.1021/jo701894v

upstream raw materials:

tert-butyl cyclohexanecarboxylate

allyl bromide

Downstream raw materials:

1-(2-oxo-ethyl)cyclohexanecarboxylic acid tert-butyl ester