N-(2-(N',N'-diethylamino)ethyl)-3-(4-phenyl-1,2,3-triazol-1-yl)-1,8-naphthalimide

Base Information

Chemical Name:N-(2-(N',N'-diethylamino)ethyl)-3-(4-phenyl-1,2,3-triazol-1-yl)-1,8-naphthalimide
CAS No.:1073775-55-9
Molecular Formula:C₂₆H₂₅N₅O₂
Molecular Weight:439.517
Hs Code.:

Synonyms:N-(2-(N',N'-diethylamino)ethyl)-3-(4-phenyl-1,2,3-triazol-1-yl)-1,8-naphthalimide

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Chemical Property of N-(2-(N',N'-diethylamino)ethyl)-3-(4-phenyl-1,2,3-triazol-1-yl)-1,8-naphthalimide

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Technology Process of N-(2-(N',N'-diethylamino)ethyl)-3-(4-phenyl-1,2,3-triazol-1-yl)-1,8-naphthalimide

There total 4 articles about N-(2-(N',N'-diethylamino)ethyl)-3-(4-phenyl-1,2,3-triazol-1-yl)-1,8-naphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1073775-49-1
3-(4-phenyl-1,2,3-triazol-1-yl)-1,8-naphthalic anhydride

: 100-36-7
N,N-diethylethylenediamine

: 1073775-55-9
N-(2-(N',N'-diethylamino)ethyl)-3-(4-phenyl-1,2,3-triazol-1-yl)-1,8-naphthalimide

Guidance literature:: In ethanol; Reflux;
DOI:10.1016/j.tet.2011.01.063

Reference yield:

: 1073775-48-0
3-azido-1,8-naphthalic anhydride

: 1073775-55-9
N-(2-(N',N'-diethylamino)ethyl)-3-(4-phenyl-1,2,3-triazol-1-yl)-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 8 h / 20 °C / Darkness

2: ethanol / Reflux

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In ethanol; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2011.01.063

Reference yield:

: 23204-38-8
3-amino-naphthalene-1,8-dicarboxylic acid-anhydride

: 1073775-55-9
N-(2-(N',N'-diethylamino)ethyl)-3-(4-phenyl-1,2,3-triazol-1-yl)-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; acetic acid; sodium nitrite / water / 1.33 h / 0 - 5 °C

1.2: 2.5 h / 0 - 20 °C

2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 8 h / 20 °C / Darkness

3.1: ethanol / Reflux

With hydrogenchloride; copper(ll) sulfate pentahydrate; acetic acid; sodium L-ascorbate; sodium nitrite; In ethanol; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2011.01.063