(4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-tetrahydro-6-<(1R,2R)-2-hydroxy-1,3-dimethyl-3-butenyl>-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone

Base Information

• Chemical Name: (4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-tetrahydro-6-<(1R,2R)-2-hydroxy-1,3-dimethyl-3-butenyl>-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone
• CAS No.: 162255-00-7
• Molecular Formula: C₂₈H₄₁NO₇
• Molecular Weight: 503.636

Synonyms:(4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-tetrahydro-6-<(1R,2R)-2-hydroxy-1,3-dimethyl-3-butenyl>-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone

Chemical Property of (4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-tetrahydro-6-<(1R,2R)-2-hydroxy-1,3-dimethyl-3-butenyl>-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone

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Technology Process of (4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-tetrahydro-6-<(1R,2R)-2-hydroxy-1,3-dimethyl-3-butenyl>-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone

There total 1 articles about (4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-tetrahydro-6-<(1R,2R)-2-hydroxy-1,3-dimethyl-3-butenyl>-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(4S)-4-benzyl-3-<(2S,4R,5S,6R)-5-methoxy-6-<(4S,5R,6R)-6-isopropenyl-2,2,5-trimethyl-1,3-dioxan-4-yl>-2,4-dimethyl-3-oxoheptanoyl>-2-oxazolidinone (124356-90-7) + trimethyl orthoformate (149-73-5) → (4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-tetrahydro-6-<(1R,2R)-2-hydroxy-1,3-dimethyl-3-butenyl>-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone (162255-00-7)

Guidance literature:

With Dowex 50; In methanol; dichloromethane; for 4h; Ambient temperature;

DOI:10.1021/ja00117a014

Reference yield: 85.0%

(4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-tetrahydro-6-<(1R,2R)-2-hydroxy-1,3-dimethyl-3-butenyl>-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone (162255-00-7) → (4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-6-<(1R,2S,3R)-2,4-dihydroxy-1,3-dimethylbutyl>tetrahydro-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone (129618-43-5)

Guidance literature:

With dimethylsulfide borane complex; In tetrahydrofuran; 1.) 0 deg C, 15 min, 2.) RT, 4 h;

DOI:10.1021/ja00117a014

Reference yield: 60.0%

(4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-tetrahydro-6-<(1R,2R)-2-hydroxy-1,3-dimethyl-3-butenyl>-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone (162255-00-7) → (4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-6-<(1R,2S,3S)-2,4-dihydroxy-1,3-dimethylbutyl>tetrahydro-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone

Guidance literature:

With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; 1.) 0 deg C, 15 min, 2.) RT, 24 h;

DOI:10.1021/ja00117a014

upstream raw materials:

(4S)-4-benzyl-3-<(2S,4R,5S,6R)-5-methoxy-6-<(4S,5R,6R)-6-isopropenyl-2,2,5-trimethyl-1,3-dioxan-4-yl>-2,4-dimethyl-3-oxoheptanoyl>-2-oxazolidinone

trimethyl orthoformate

Downstream raw materials:

(4S)-4-benzyl-3-<(2S)-2-<(2R,3R,4S,5R,6R)-6-<(1R,2S,3R)-2,4-dihydroxy-1,3-dimethylbutyl>tetrahydro-2,4-dimethoxy-3,5-dimethyl-2H-pyran-2-yl>propionyl>-2-oxazolidinone

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