(-)-(2S,3S,1'S)-3-[1'-benzoyloxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane

Base Information

Chemical Name:(-)-(2S,3S,1'S)-3-[1'-benzoyloxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane
CAS No.:1308348-20-0
Molecular Formula:C₃₂H₃₁NO₃
Molecular Weight:477.603
Hs Code.:

Synonyms:(-)-(2S,3S,1'S)-3-[1'-benzoyloxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(2S,3S,1'S)-3-[1'-benzoyloxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane

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Technology Process of (-)-(2S,3S,1'S)-3-[1'-benzoyloxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane

There total 1 articles about (-)-(2S,3S,1'S)-3-[1'-benzoyloxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: (-)-(2S,3S,1'S)-3-[1'-hydroxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane

: 98-88-4
benzoyl chloride

: 1308348-20-0
(-)-(2S,3S,1'S)-3-[1'-benzoyloxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane

Guidance literature:: (-)-(2S,3S,1'S)-3-[1'-hydroxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane; With n-butyllithium; In tetrahydrofuran; hexane; at -75 ℃; for 0.666667h; Inert atmosphere;

benzoyl chloride; In tetrahydrofuran; hexane; at -75 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.molcata.2011.02.008

Reference yield: 87.0%

: 1308348-20-0
(-)-(2S,3S,1'S)-3-[1'-benzoyloxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane

: 1308348-24-4
(2S,3R)-4-amino-3-benzoyloxy-2-benzylbutan-1-ol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; at 30 ℃; for 16h; under 7500.75 Torr;
DOI:10.1016/j.molcata.2011.02.008

Reference yield: 70.0%

: 1308348-20-0
(-)-(2S,3S,1'S)-3-[1'-benzoyloxy-2'-(dibenzylamino)ethyl]-2-phenyloxetane

: 1308348-26-6
(2S,3R)-4-amino-2-benzyl-3-benzoylbutan-1-ol hydrochloride

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In dichloromethane; at 45 ℃; for 24h; under 7500.75 Torr;
DOI:10.1016/j.molcata.2011.02.008