C₂₈H₂₈N₆S

Base Information

• Chemical Name: C₂₈H₂₈N₆S
• CAS No.: 1312610-06-2
• Molecular Formula: C₂₈H₂₈N₆S
• Molecular Weight: 480.637

Synonyms:C₂₈H₂₈N₆S

Chemical Property of C₂₈H₂₈N₆S

Chemical Property:

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Technology Process of C₂₈H₂₈N₆S

There total 13 articles about C₂₈H₂₈N₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C38H44N6O4S (1312610-05-1) → C28H28N6S (1312610-06-2)

Guidance literature:

With hydrogenchloride; In methanol; at 20 ℃;

Reference yield:

3-methoxy-2-hydroxybenzaldehyde (148-53-8) → C28H28N6S (1312610-06-2)

Guidance literature:

Multi-step reaction with 13 steps

1.1: potassium hydroxide / water; tetrahydrofuran / 0 - 20 °C

2.1: diphenylether / 240 - 250 °C / Inert atmosphere

3.1: sodium hydroxide; water / methanol / 2 h / Inert atmosphere; Reflux

4.1: sodium hydroxide / water / 4 h / 100 °C

4.2: 20 °C / pH 4 - 5

5.1: sodium hydroxide / diphenylether; water / 6 h / 100 °C

5.2: 20 °C / pH 4 - 5

6.1: copper; quinoline / 1.5 h / 210 - 220 °C / Inert atmosphere

7.1: bromine / tetrachloromethane / 2.5 h / 0 °C

8.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 80 °C / Inert atmosphere

9.1: boron tribromide / dichloromethane / 2 h / -70 - 20 °C

9.2: Cooling with ice

10.1: triethylamine / dichloromethane / 3 h / -40 - 20 °C

11.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 80 °C / Inert atmosphere

12.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

13.1: hydrogenchloride / methanol / 20 °C

With quinoline; hydrogenchloride; water; bromine; potassium acetate; boron tribromide; copper; sodium carbonate; triethylamine; potassium hydroxide; sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; methanol; tetrachloromethane; diphenylether; ethanol; dichloromethane; water; toluene; 8.1: Suzuki Coupling / 12.1: Suzuki Coupling;

Reference yield:

7-methoxybenzothiophene (88791-08-6) → C28H28N6S (1312610-06-2)

Guidance literature:

Multi-step reaction with 7 steps

1.1: bromine / tetrachloromethane / 2.5 h / 0 °C

2.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 80 °C / Inert atmosphere

3.1: boron tribromide / dichloromethane / 2 h / -70 - 20 °C

3.2: Cooling with ice

4.1: triethylamine / dichloromethane / 3 h / -40 - 20 °C

5.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 80 °C / Inert atmosphere

6.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

7.1: hydrogenchloride / methanol / 20 °C

With hydrogenchloride; bromine; potassium acetate; boron tribromide; sodium carbonate; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; methanol; tetrachloromethane; ethanol; dichloromethane; toluene; 2.1: Suzuki Coupling / 6.1: Suzuki Coupling;

upstream raw materials:

3-methoxy-2-hydroxybenzaldehyde

7-methoxybenzothiophene

O-(2-formyl-6-methoxyphenyl)-N,N-dimethylthiocarbamate

S-(2-formyl-6-methoxyphenyl)-N,N-dimethylthiocarbamate

Downstream raw materials:

C₄₂H₅₀N₈O₆S

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