(3aR,4S,6aS)-4-[4-(1-Benzyloxy-hexyl)-phenyl]-hexahydro-cyclopenta[b]furan-2-one

Base Information

Chemical Name:(3aR,4S,6aS)-4-[4-(1-Benzyloxy-hexyl)-phenyl]-hexahydro-cyclopenta[b]furan-2-one
CAS No.:879098-69-8
Molecular Formula:C₂₆H₃₂O₃
Molecular Weight:392.538
Hs Code.:

Synonyms:(3aR,4S,6aS)-4-[4-(1-Benzyloxy-hexyl)-phenyl]-hexahydro-cyclopenta[b]furan-2-one

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Chemical Property of (3aR,4S,6aS)-4-[4-(1-Benzyloxy-hexyl)-phenyl]-hexahydro-cyclopenta[b]furan-2-one

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Technology Process of (3aR,4S,6aS)-4-[4-(1-Benzyloxy-hexyl)-phenyl]-hexahydro-cyclopenta[b]furan-2-one

There total 6 articles about (3aR,4S,6aS)-4-[4-(1-Benzyloxy-hexyl)-phenyl]-hexahydro-cyclopenta[b]furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 879098-90-5
thiocarbonic acid O-{4-[4-(1-benzyloxy-hexyl)-phenyl]-2-oxo-hexahydro-cyclopenta[b]furan-5-yl} ester O-phenyl ester

: 879098-69-8
(3aR,4S,6aS)-4-[4-(1-Benzyloxy-hexyl)-phenyl]-hexahydro-cyclopenta[b]furan-2-one

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In toluene; for 1h; Heating;
DOI:10.1021/ja057560o

Reference yield:

: 879098-65-4
Acetic acid (1R,4S)-4-(1-butoxy-2-iodo-ethoxy)-cyclopent-2-enyl ester

: 879098-69-8
(3aR,4S,6aS)-4-[4-(1-Benzyloxy-hexyl)-phenyl]-hexahydro-cyclopenta[b]furan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: CoCl₂; (R,R)-1,2-bis(dimethylamino)cyclohexane / tetrahydrofuran / 0.25 h / 25 °C

1.2: 54 percent / Jones reagent / acetone / 20 °C

2.1: 85 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

3.1: pyridine; N,N-dimethyl-4-aminopyridine / CH₂Cl₂ / 12 h / 20 °C

4.1: 235 mg / AIBN; (Me₃Si)3SiH / toluene / 1 h / Heating

With pyridine; dmap; 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; (1R,2R)-bis(dimethylamino)cyclohexane; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja057560o

Reference yield:

: C₁₉H₂₃BrMgO

: 879098-69-8
(3aR,4S,6aS)-4-[4-(1-Benzyloxy-hexyl)-phenyl]-hexahydro-cyclopenta[b]furan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: CoCl₂; (R,R)-1,2-bis(dimethylamino)cyclohexane / tetrahydrofuran / 0.25 h / 25 °C

1.2: 54 percent / Jones reagent / acetone / 20 °C

2.1: 85 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

3.1: pyridine; N,N-dimethyl-4-aminopyridine / CH₂Cl₂ / 12 h / 20 °C

4.1: 235 mg / AIBN; (Me₃Si)3SiH / toluene / 1 h / Heating

With pyridine; dmap; 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; (1R,2R)-bis(dimethylamino)cyclohexane; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja057560o