[(S)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-carbamic acid methyl ester

Base Information

Chemical Name:[(S)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-carbamic acid methyl ester
CAS No.:147671-72-5
Molecular Formula:C₂₇H₄₃NO₄Si₂
Molecular Weight:501.814
Hs Code.:

Synonyms:[(S)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-carbamic acid methyl ester

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Chemical Property of [(S)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-carbamic acid methyl ester

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Technology Process of [(S)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-carbamic acid methyl ester

There total 5 articles about [(S)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-carbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96854-24-9
(S)-N-(Methoxycarbonyl)serine Methyl Ester

: 147671-72-5
[(S)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N, 4-dimethylaminopyridine / CH₂Cl₂

2: NaBH₄ / methanol

3: imidazole / dimethylformamide

With 1H-imidazole; dmap; sodium tetrahydroborate; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39930000125

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 147671-72-5
[(S)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N, 4-dimethylaminopyridine / CH₂Cl₂

2: NaBH₄ / methanol

3: imidazole / dimethylformamide

With 1H-imidazole; dmap; sodium tetrahydroborate; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39930000125

Reference yield:

: (S)-3-hydroxy-2-((methoxycarbonyl)amino)propanoic acid

: 147671-72-5
[(S)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether

2: Et₃N, 4-dimethylaminopyridine / CH₂Cl₂

3: NaBH₄ / methanol

4: imidazole / dimethylformamide

With 1H-imidazole; dmap; sodium tetrahydroborate; triethylamine; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39930000125