N-fluoren-9-ylmethoxycarbonyl-L-phenylalanine 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamide

Base Information

Chemical Name:N-fluoren-9-ylmethoxycarbonyl-L-phenylalanine 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamide
CAS No.:1174889-98-5
Molecular Formula:C₃₈H₄₀N₂O₁₂
Molecular Weight:716.742
Hs Code.:

Synonyms:N-fluoren-9-ylmethoxycarbonyl-L-phenylalanine 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-fluoren-9-ylmethoxycarbonyl-L-phenylalanine 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamide

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Technology Process of N-fluoren-9-ylmethoxycarbonyl-L-phenylalanine 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamide

There total 2 articles about N-fluoren-9-ylmethoxycarbonyl-L-phenylalanine 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 41355-50-4,51642-81-0,58484-22-3,70128-27-7,70145-20-9,94482-21-0,98300-76-6
2,3,4,6-tetra-O-acetyl-D-glucosyl-1-amine

: 35661-40-6
N-Fmoc L-Phe

: 1174889-98-5
N-fluoren-9-ylmethoxycarbonyl-L-phenylalanine 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamide

Guidance literature:: With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine; In ethyl acetate; at 20 ℃; for 16h; Reagent/catalyst; Solvent;
DOI:10.1007/s10989-017-9614-4

Reference yield: 36.0%

: 1174889-96-3
S-2,4,6-trimethoxybenzyl N-Fluoren-9-ylmethoxycarbonyl-L-thiophenylalaninate

: 104974-80-3
Acetic acid (2R,3R,4S,5R,6R)-3,5-diacetoxy-2-acetoxymethyl-6-isocyanato-tetrahydro-pyran-4-yl ester

: 1174889-98-5
N-fluoren-9-ylmethoxycarbonyl-L-phenylalanine 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamide

Guidance literature:: S-2,4,6-trimethoxybenzyl N-Fluoren-9-ylmethoxycarbonyl-L-thiophenylalaninate; With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

Acetic acid (2R,3R,4S,5R,6R)-3,5-diacetoxy-2-acetoxymethyl-6-isocyanato-tetrahydro-pyran-4-yl ester; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1021/ol901370y