8--1,4-dioxaspiro<4.5>decan

Base Information

Chemical Name:8--1,4-dioxaspiro<4.5>decan
CAS No.:96370-95-5
Molecular Formula:C₂₃H₂₆O₄
Molecular Weight:366.457
Hs Code.:

8-<Bis-(4-methoxyphenyl)-methylen>-1,4-dioxaspiro<4.5>decan

Synonyms:8--1,4-dioxaspiro<4.5>decan

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8--1,4-dioxaspiro<4.5>decan

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Technology Process of 8--1,4-dioxaspiro<4.5>decan

There total 3 articles about 8--1,4-dioxaspiro<4.5>decan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 5720-07-0
4-methoxyphenylboronic acid

: 175020-73-2
4-(dibromomethylene)cyclohexanone ethylene ketal

: 96370-95-5
8--1,4-dioxaspiro<4.5>decan

Guidance literature:: With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; water; at 65 ℃;
DOI:10.1055/s-2001-10776

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 90-96-0
bis(p-methoxyphenyl)methanone

: 96370-95-5
8--1,4-dioxaspiro<4.5>decan

: 94968-12-4
4-(Bis-(4-methoxy-phenyl)-methylen)-cyclohexanon

Guidance literature:: With titanium tetrachloride; zinc; In tetrahydrofuran; for 4.5h; Overall yield = 8.50 g; Reflux;
DOI:10.1016/j.bmc.2015.09.046