[Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₃

Base Information

Chemical Name:[Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₃
CAS No.:884050-49-1
Molecular Formula:C₂₆H₃₀Cl₃F₂FeN₂
Molecular Weight:570.74
Hs Code.:

[Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl<sub>3</sub>

Synonyms:[Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₃

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Chemical Property of [Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₃

Chemical Property:

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Technology Process of [Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₃

There total 1 articles about [Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 884050-45-7
Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy

: 7705-08-0
iron(III) chloride

: 884050-49-1
[Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₃

Guidance literature:: In dichloromethane; soln. stirred for 24 h; soln. filtered, solvent removed in vacuo; washed with pentane;
DOI:10.1002/anie.200502985

Reference yield:

: 884050-49-1
[Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₃

: 60779-09-1
1-phenylethylmagnesium chloride

: 884050-47-9
[Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₂

Guidance literature:: With ONC(CH₃)2C₃H₆C(CH₃)2; In tetrahydrofuran; byproducts: MgCl2, C6H5CH(CH3)ONC(CH3)2C3H6C(CH3)2; (N2); std. Schlenk technique; soln. of N-oxide in THF was added dropwiseto soln. of Fe complex in THF at -78°C; soln. of Mg compd. in TH F was added;
DOI:10.1021/om700395h

Reference yield:

: 884050-49-1
[Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₃

: 6921-34-2
benzylmagnesium chloride

: 884050-47-9
[Cy-N=C(para-fluorophenyl)-C(para-fluorophenyl)=N-Cy]FeCl₂

Guidance literature:: In tetrahydrofuran; byproducts: (C6H5CH2)2, MgCl2; (N2); std. Schlenk technique; soln. of Mg compd. in THF was added dropwise to soln. of Fe complex in THF at -78°C;
DOI:10.1021/om700395h