N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid methyl ester

Base Information

Chemical Name:N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid methyl ester
CAS No.:1449061-28-2
Molecular Formula:C₂₂H₂₈ClNO₄Si
Molecular Weight:434.007
Hs Code.:

Synonyms:N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid methyl ester

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Chemical Property of N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid methyl ester

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Technology Process of N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid methyl ester

There total 1 articles about N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 220848-41-9
2-chloro-4-[[[(3-hydroxyphenyl)methyl]amino]carbonyl]benzoic acid methyl ester

: 1449061-28-2
N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid methyl ester

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1449061-28-2
N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid methyl ester

: 1449061-29-3
N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid

Guidance literature:: With trimethyltin(IV) hydroxide; In 1,2-dichloro-ethane; at 80 ℃; for 8h;

Reference yield:

: 1449061-28-2
N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid methyl ester

: 1449061-30-6
(S)-2-{4-[3-(tert-butyldimethylsilanyloxy)benzylcarbamoyl]-2-chlorobenzoylamino}-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 8 h / 80 °C

2: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trimethyltin(IV) hydroxide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;