N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid

Base Information

Chemical Name:N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid
CAS No.:1449061-29-3
Molecular Formula:C₂₁H₂₆ClNO₄Si
Molecular Weight:419.98
Hs Code.:

Synonyms:N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid

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Chemical Property of N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid

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Technology Process of N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid

There total 3 articles about N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449061-28-2
N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid methyl ester

: 1449061-29-3
N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid

Guidance literature:: With trimethyltin(IV) hydroxide; In 1,2-dichloro-ethane; at 80 ℃; for 8h;

Reference yield:

: 220848-41-9
2-chloro-4-[[[(3-hydroxyphenyl)methyl]amino]carbonyl]benzoic acid methyl ester

: 1449061-29-3
N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 8 h / 80 °C

With 1H-imidazole; trimethyltin(IV) hydroxide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1449061-29-3
N-[3-(tert-butyldimethylsilanyloxy)benzyl]-2-chloroterephthalamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 8 h / 80 °C

With 1H-imidazole; trimethyltin(IV) hydroxide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;