Technology Process of C36H33N3O6
There total 5 articles about C36H33N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 89 percent / LiBH4 / tetrahydrofuran / 0.33 h
2: 71 percent / pyridinium trifluoroacetate, 1,3-dicyclohexylcarbodiimide / benzene; dimethylsulfoxide / 9 h / Ambient temperature
3: 85 percent / BF3*OEt2 / diethyl ether / 24 h / 25 - 30 °C
4: 95 percent / NaBH4 / methanol; CH2Cl2; CHCl3 / 0.08 h
5: 1.) NaH / 1) THF, 25 min; 2) THF, 50 min
With
sodium tetrahydroborate; lithium borohydride; boron trifluoride diethyl etherate; pyridinium trifluroacetate; sodium hydride; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; dimethyl sulfoxide; benzene;
DOI:10.1021/ja971304x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95 percent / NaBH4 / methanol; CH2Cl2; CHCl3 / 0.08 h
2: 1.) NaH / 1) THF, 25 min; 2) THF, 50 min
With
sodium tetrahydroborate; sodium hydride;
In
methanol; dichloromethane; chloroform;
DOI:10.1021/ja971304x
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 71 percent / pyridinium trifluoroacetate, 1,3-dicyclohexylcarbodiimide / benzene; dimethylsulfoxide / 9 h / Ambient temperature
2: 85 percent / BF3*OEt2 / diethyl ether / 24 h / 25 - 30 °C
3: 95 percent / NaBH4 / methanol; CH2Cl2; CHCl3 / 0.08 h
4: 1.) NaH / 1) THF, 25 min; 2) THF, 50 min
With
sodium tetrahydroborate; boron trifluoride diethyl etherate; pyridinium trifluroacetate; sodium hydride; dicyclohexyl-carbodiimide;
In
methanol; diethyl ether; dichloromethane; chloroform; dimethyl sulfoxide; benzene;
DOI:10.1021/ja971304x