C₆H₁₁CH(Si(CH₃)3)B(OCH₂)2

Base Information

Chemical Name:C₆H₁₁CH(Si(CH₃)3)B(OCH₂)2
CAS No.:72823-96-2
Molecular Formula:C₁₂H₂₅BO₂Si
Molecular Weight:240.226
Hs Code.:

C<sub>6</sub>H<sub>11</sub>CH(Si(CH<sub>3</sub>)3)B(OCH<sub>2</sub>)2

Synonyms:C₆H₁₁CH(Si(CH₃)3)B(OCH₂)2

Suppliers and Price of C₆H₁₁CH(Si(CH₃)3)B(OCH₂)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆H₁₁CH(Si(CH₃)3)B(OCH₂)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆H₁₁CH(Si(CH₃)3)B(OCH₂)2

There total 2 articles about C₆H₁₁CH(Si(CH₃)3)B(OCH₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 66217-60-5
2-cyclohexyl-1,3,2-dioxaborolane

: 2344-80-1
Chloromethyltrimethylsilane

: 72823-96-2
C₆H₁₁CH(Si(CH₃)3)B(OCH₂)2

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; sec-BuLi was added dropwise at -78°C to Me3SiCH2Cl in THF, TMEDAadded, stirred 45 min at -78°C, warmed to -55°C, boronatein THF was added, stirred 10 min at -55°C, cooled to -78°C, warmed to 25°C overnight; 2 M ice-cold HCl was added, mixt. extd. with 5:1 Et2O-CH2Cl2, org. phase concd. in vacuo, residue was treated with HOCH2CH2OH and hexane or benzene, refluxed with a Dean-Stark trap, dried over CaCl2, evapd., residuedistilled in vacuo; elem. anal.;
DOI:10.1021/om00074a005

Reference yield: 81.0%

: 66217-60-5
2-cyclohexyl-1,3,2-dioxaborolane

: 63830-85-3
chloro(trimethylsilyl)methyl lithium

: 72823-96-2
C₆H₁₁CH(Si(CH₃)3)B(OCH₂)2

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; (Ar); to soln. of Me3SiCHLiCl was added boronic ester at -55°C, after 10 min was cooled with dry ice, mixt. was allowed to warm up slowly to room temp. and stirred overnight; mixt. was treated with aq. HCl and extd. with ether/CH2Cl2 5:1; esters were treated with ethylene glycol and distd.; elem. anal.;
DOI:10.1016/S0022-328X(00)83500-7