Technology Process of C24H28N6O
There total 8 articles about C24H28N6O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
tetrahydrofuran; thiophene; methanol; di-isopropyl ether;
at 50 ℃;
under 57003.8 Torr;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: trichlorophosphate / 2 h / 100 °C
1.2: Cooling with ice
2.1: sodium carbonate / triphenylphosphine; palladium diacetate / 1,2-dimethoxyethane; water / 4 h / Reflux
3.1: caesium carbonate / tris-(dibenzylideneacetone)dipalladium(0); XPhos / water; tert-butyl alcohol / 1 h / 105 °C / Inert atmosphere; microwave irradiation
4.1: manganese(IV) oxide / tetrahydrofuran / 18 h / 20 °C
5.1: hydrogen / palladium 10% on activated carbon / di-isopropyl ether; thiophene; tetrahydrofuran; methanol / 50 °C / 57003.8 Torr / Inert atmosphere
With
manganese(IV) oxide; hydrogen; sodium carbonate; caesium carbonate; trichlorophosphate;
tris-(dibenzylideneacetone)dipalladium(0); palladium 10% on activated carbon; palladium diacetate; triphenylphosphine; XPhos;
In
tetrahydrofuran; thiophene; methanol; 1,2-dimethoxyethane; di-isopropyl ether; water; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium carbonate / triphenylphosphine; palladium diacetate / 1,2-dimethoxyethane; water / 4 h / Reflux
2: caesium carbonate / tris-(dibenzylideneacetone)dipalladium(0); XPhos / water; tert-butyl alcohol / 1 h / 105 °C / Inert atmosphere; microwave irradiation
3: manganese(IV) oxide / tetrahydrofuran / 18 h / 20 °C
4: hydrogen / palladium 10% on activated carbon / di-isopropyl ether; thiophene; tetrahydrofuran; methanol / 50 °C / 57003.8 Torr / Inert atmosphere
With
manganese(IV) oxide; hydrogen; sodium carbonate; caesium carbonate;
tris-(dibenzylideneacetone)dipalladium(0); palladium 10% on activated carbon; palladium diacetate; triphenylphosphine; XPhos;
In
tetrahydrofuran; thiophene; methanol; 1,2-dimethoxyethane; di-isopropyl ether; water; tert-butyl alcohol;