Technology Process of C17H25NO3
There total 6 articles about C17H25NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium acetate; sodium tris(acetoxy)borohydride;
In
dichloromethane;
at 0 - 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 - 20 °C
1.2: 4 h / 0 °C
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2.08 h / 0 - 20 °C
4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C
5.1: sodium acetate; sodium tris(acetoxy)borohydride / dichloromethane / 0 - 20 °C
With
lithium aluminium tetrahydride; sodium acetate; sodium tris(acetoxy)borohydride; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; mineral oil;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 2.08 h / 0 - 20 °C
3: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C
4: sodium acetate; sodium tris(acetoxy)borohydride / dichloromethane / 0 - 20 °C
With
lithium aluminium tetrahydride; sodium acetate; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;