rel-(3R,3aS,7aR)-2-benzyl-3-ethoxy-2,3,3a,4,7,7a-hexahydro-1-isoindolone

Base Information

Chemical Name:rel-(3R,3aS,7aR)-2-benzyl-3-ethoxy-2,3,3a,4,7,7a-hexahydro-1-isoindolone
CAS No.:95455-15-5
Molecular Formula:C₁₇H₂₁NO₂
Molecular Weight:271.359
Hs Code.:

Synonyms:rel-(3R,3aS,7aR)-2-benzyl-3-ethoxy-2,3,3a,4,7,7a-hexahydro-1-isoindolone

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Chemical Property of rel-(3R,3aS,7aR)-2-benzyl-3-ethoxy-2,3,3a,4,7,7a-hexahydro-1-isoindolone

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Technology Process of rel-(3R,3aS,7aR)-2-benzyl-3-ethoxy-2,3,3a,4,7,7a-hexahydro-1-isoindolone

There total 3 articles about rel-(3R,3aS,7aR)-2-benzyl-3-ethoxy-2,3,3a,4,7,7a-hexahydro-1-isoindolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 64-17-5
ethanol

: 66050-03-1
cis-2-benzyl-1,3,3a,4,7,7a-hexahydro-1,3-isoindoledione

: 95455-15-5
rel-(3R,3aS,7aR)-2-benzyl-3-ethoxy-2,3,3a,4,7,7a-hexahydro-1-isoindolone

Guidance literature:: With hydrogenchloride; sodium tetrahydroborate; at 0 - 5 ℃; for 4h;
DOI:10.1016/S0040-4020(01)86638-2

Reference yield:

: 100-44-7
benzyl chloride

: 95455-15-5
rel-(3R,3aS,7aR)-2-benzyl-3-ethoxy-2,3,3a,4,7,7a-hexahydro-1-isoindolone

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone

2: 1.) NaBH₄

With sodium tetrahydroborate; potassium carbonate; In acetone;
DOI:10.1016/S0040-4039(01)91310-3

Reference yield:

: 1469-48-3,565227-54-5
cis-1,2,3,6-Tetrahydrophthalimide

: 95455-15-5
rel-(3R,3aS,7aR)-2-benzyl-3-ethoxy-2,3,3a,4,7,7a-hexahydro-1-isoindolone

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone

2: 1.) NaBH₄

With sodium tetrahydroborate; potassium carbonate; In acetone;
DOI:10.1016/S0040-4039(01)91310-3