(S)-methyl 3-(5-bromo-2-fluorophenyl)-3-((R)-1,1-dimethylethylsulfinamido)-4-fluorobutanoate

Base Information

Chemical Name:(S)-methyl 3-(5-bromo-2-fluorophenyl)-3-((R)-1,1-dimethylethylsulfinamido)-4-fluorobutanoate
CAS No.:1624605-44-2
Molecular Formula:C₁₅H₂₀BrF₂NO₃S
Molecular Weight:412.296
Hs Code.:

Synonyms:(S)-methyl 3-(5-bromo-2-fluorophenyl)-3-((R)-1,1-dimethylethylsulfinamido)-4-fluorobutanoate

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Chemical Property of (S)-methyl 3-(5-bromo-2-fluorophenyl)-3-((R)-1,1-dimethylethylsulfinamido)-4-fluorobutanoate

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Technology Process of (S)-methyl 3-(5-bromo-2-fluorophenyl)-3-((R)-1,1-dimethylethylsulfinamido)-4-fluorobutanoate

There total 3 articles about (S)-methyl 3-(5-bromo-2-fluorophenyl)-3-((R)-1,1-dimethylethylsulfinamido)-4-fluorobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.6%

: chlorotitanium triisopropoxide

: (R,E)-N-(1-(5-bromo-2-fluorophenyl)-2-fluoroethylidene)-2-methylpropane-2-sulfinamide

: 1624605-44-2
(S)-methyl 3-(5-bromo-2-fluorophenyl)-3-((R)-1,1-dimethylethylsulfinamido)-4-fluorobutanoate

Guidance literature:: With n-butyllithium; ammonium chloride; In tetrahydrofuran; [⁽²⁾H₆]acetone; acetic acid methyl ester;

Reference yield:

: 1600511-51-0
1-(5-bromo-2-fluorophenyl)-2-fluoroethan-1-one

: 1624605-44-2
(S)-methyl 3-(5-bromo-2-fluorophenyl)-3-((R)-1,1-dimethylethylsulfinamido)-4-fluorobutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; ethyl acetate; water

2: n-butyllithium; ammonium chloride / tetrahydrofuran; acetic acid methyl ester; [⁽²⁾H₆]acetone

With n-butyllithium; ammonium chloride; In tetrahydrofuran; [⁽²⁾H₆]acetone; acetic acid methyl ester; water; ethyl acetate;

Reference yield:

: 116272-41-4
4-bromo-1-fluoro-2-iodobenzene

: 1624605-44-2
(S)-methyl 3-(5-bromo-2-fluorophenyl)-3-((R)-1,1-dimethylethylsulfinamido)-4-fluorobutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium; ammonium chloride / tetrahydrofuran; ethyl acetate

2: tetrahydrofuran; ethyl acetate; water

3: n-butyllithium; ammonium chloride / tetrahydrofuran; acetic acid methyl ester; [⁽²⁾H₆]acetone

With n-butyllithium; ammonium chloride; In tetrahydrofuran; [⁽²⁾H₆]acetone; acetic acid methyl ester; water; ethyl acetate;