p-bromophenacyl acrylate

Base Information

Chemical Name:p-bromophenacyl acrylate
CAS No.:67028-16-4
Molecular Formula:C₁₁H₉BrO₃
Molecular Weight:269.095
Hs Code.:

Synonyms:p-bromophenacyl acrylate

Suppliers and Price of p-bromophenacyl acrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-bromophenacyl acrylate

Chemical Property:

Purity/Quality:

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Technology Process of p-bromophenacyl acrylate

There total 4 articles about p-bromophenacyl acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.6%

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 79-10-7
acrylic acid

: 67028-16-4
p-bromophenacyl acrylate

Guidance literature:: With potassium fluoride; In N,N-dimethyl-formamide; for 0.25h; Ambient temperature;
DOI:10.1021/ac50064a047

Reference yield:

: 67028-15-3
3-Hydroxy-propionsaeure-(4-brom-phenacylester)

: 67028-16-4
p-bromophenacyl acrylate

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/ja00478a041

Reference yield:

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 67028-16-4
p-bromophenacyl acrylate

Guidance literature:: Multi-step reaction with 3 steps

1: (i) SOCl₂, Py, CH₂Cl₂, (ii) RuO₂, aq. NaIO₄, HIO₄, tBuOH, (iii) /BRN= 607604/, 18-crown-6, MeCN

2: (i) K₂CO₃, MeOH, (ii) 18-crown-6, MeCN

3: MeSO₂Cl, Et₃N / CH₂Cl₂

With methanesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/ja00478a041