-5-(4-nitro-phenylazo)-phenyl>--phenyl>-ether

Base Information

• Chemical Name: -5-(4-nitro-phenylazo)-phenyl>--phenyl>-ether
• CAS No.: 97657-13-1
• Molecular Formula: C₃₄H₃₁N₉O₃
• Molecular Weight: 613.679
• Mol file: 97657-13-1.mol

Synonyms:-5-(4-nitro-phenylazo)-phenyl>--phenyl>-ether

Chemical Property of -5-(4-nitro-phenylazo)-phenyl>--phenyl>-ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of -5-(4-nitro-phenylazo)-phenyl>--phenyl>-ether

There total 4 articles about -5-(4-nitro-phenylazo)-phenyl>--phenyl>-ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(2-aminophenyl)ether (24878-25-9) + 4-nitrobenzenediazonium chloride (100-05-0) + N,N-dimethyl-aniline (121-69-7,77733-26-7) → -5-(4-nitro-phenylazo)-phenyl>--phenyl>-ether (97657-13-1)

Guidance literature:

Multistep reaction; (i), (ii) aq. HCl, NaNO₂, (iii) /BRN= 507140/;

DOI:10.1021/jo01058a532

Reference yield:

potassium 2-nitrophenoxide (824-38-4) → -5-(4-nitro-phenylazo)-phenyl>--phenyl>-ether (97657-13-1)

Guidance literature:

Multi-step reaction with 3 steps

1: dimethylformamide

2: H₂ / Pd-C

3: (i), (ii) aq. HCl, NaNO₂, (iii) /BRN= 507140/

With hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;

DOI:10.1021/jo01058a532

Reference yield:

2-Chloronitrobenzene (88-73-3) → -5-(4-nitro-phenylazo)-phenyl>--phenyl>-ether (97657-13-1)

Guidance literature:

Multi-step reaction with 3 steps

1: dimethylformamide

2: H₂ / Pd-C

3: (i), (ii) aq. HCl, NaNO₂, (iii) /BRN= 507140/

With hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;

DOI:10.1021/jo01058a532

upstream raw materials:

bis(2-aminophenyl)ether

4-nitrobenzenediazonium chloride

N,N-dimethyl-aniline

bis(2-nitrophenyl)ether