[3-(3-oxopropyl)phenyl]acetic acid methyl ester

Base Information

Chemical Name:[3-(3-oxopropyl)phenyl]acetic acid methyl ester
CAS No.:1254580-40-9
Molecular Formula:C₁₂H₁₄O₃
Molecular Weight:206.241
Hs Code.:

Synonyms:[3-(3-oxopropyl)phenyl]acetic acid methyl ester

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Chemical Property of [3-(3-oxopropyl)phenyl]acetic acid methyl ester

Chemical Property:

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Technology Process of [3-(3-oxopropyl)phenyl]acetic acid methyl ester

There total 5 articles about [3-(3-oxopropyl)phenyl]acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1254580-39-6
[3-(3-hydroxypropyl)phenyl]acetic acid methyl ester

: 1254580-40-9
[3-(3-oxopropyl)phenyl]acetic acid methyl ester

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 0 - 20 ℃; for 3.33333h; Molecular sieve; Inert atmosphere;

Reference yield:

: 1878-67-7
3-Bromophenylacetic acid

: 1254580-40-9
[3-(3-oxopropyl)phenyl]acetic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / 3 h / Reflux

2: sodium iodide; copper(l) iodide; N,N`-dimethylethylenediamine / tert-butyl alcohol / 1 h / 145 - 150 °C / Inert atmosphere; microwave irradiation

3: diethylamine; triphenylphosphine; copper(l) iodide; palladium dichloride / 45 °C / Inert atmosphere

4: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C

5: pyridinium chlorochromate / dichloromethane / 3.33 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

With copper(l) iodide; hydrogen; toluene-4-sulfonic acid; diethylamine; triphenylphosphine; pyridinium chlorochromate; sodium iodide; palladium dichloride; N,N`-dimethylethylenediamine; palladium 10% on activated carbon; In ethanol; dichloromethane; tert-butyl alcohol;

Reference yield:

: 502649-73-2
methyl 3-iodophenyl acetic acid

: 1254580-40-9
[3-(3-oxopropyl)phenyl]acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diethylamine; triphenylphosphine; copper(l) iodide; palladium dichloride / 45 °C / Inert atmosphere

2: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C

3: pyridinium chlorochromate / dichloromethane / 3.33 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

With copper(l) iodide; hydrogen; diethylamine; triphenylphosphine; pyridinium chlorochromate; palladium dichloride; palladium 10% on activated carbon; In ethanol; dichloromethane;