4-O-(6-O-benzyl-3,4-O-isopropylidene-2-O-p-methoxybenzyl-β-D-talopyranosyl)-2,3:5,6-di-O-isopropylidenealdehydo-D-glucose dimethyl acetal

Base Information

Chemical Name:4-O-(6-O-benzyl-3,4-O-isopropylidene-2-O-p-methoxybenzyl-β-D-talopyranosyl)-2,3:5,6-di-O-isopropylidenealdehydo-D-glucose dimethyl acetal
CAS No.:1590392-10-1
Molecular Formula:C₃₈H₅₄O₁₃
Molecular Weight:718.839
Hs Code.:

Synonyms:4-O-(6-O-benzyl-3,4-O-isopropylidene-2-O-p-methoxybenzyl-β-D-talopyranosyl)-2,3:5,6-di-O-isopropylidenealdehydo-D-glucose dimethyl acetal

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Chemical Property of 4-O-(6-O-benzyl-3,4-O-isopropylidene-2-O-p-methoxybenzyl-β-D-talopyranosyl)-2,3:5,6-di-O-isopropylidenealdehydo-D-glucose dimethyl acetal

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Technology Process of 4-O-(6-O-benzyl-3,4-O-isopropylidene-2-O-p-methoxybenzyl-β-D-talopyranosyl)-2,3:5,6-di-O-isopropylidenealdehydo-D-glucose dimethyl acetal

There total 4 articles about 4-O-(6-O-benzyl-3,4-O-isopropylidene-2-O-p-methoxybenzyl-β-D-talopyranosyl)-2,3:5,6-di-O-isopropylidenealdehydo-D-glucose dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₄₈O₁₃

: 100-39-0
benzyl bromide

: 1590392-10-1
4-O-(6-O-benzyl-3,4-O-isopropylidene-2-O-p-methoxybenzyl-β-D-talopyranosyl)-2,3:5,6-di-O-isopropylidenealdehydo-D-glucose dimethyl acetal

Guidance literature:: C₃₁H₄₈O₁₃; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 0.333333h;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 12h;
DOI:10.1016/j.carres.2014.01.020

Reference yield:

: C₃₅H₅₆O₁₄

: 1590392-10-1
4-O-(6-O-benzyl-3,4-O-isopropylidene-2-O-p-methoxybenzyl-β-D-talopyranosyl)-2,3:5,6-di-O-isopropylidenealdehydo-D-glucose dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / dichloromethane; water

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 - 20 °C

2.2: 12 h / 0 - 20 °C

With hydrogenchloride; sodium hydride; In dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.carres.2014.01.020

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1590392-10-1
4-O-(6-O-benzyl-3,4-O-isopropylidene-2-O-p-methoxybenzyl-β-D-talopyranosyl)-2,3:5,6-di-O-isopropylidenealdehydo-D-glucose dimethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: hydrogenchloride / dichloromethane; water

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 - 20 °C

3.2: 12 h / 0 - 20 °C

With hydrogenchloride; sodium hydride; In dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.carres.2014.01.020