5,10,15,20-tetrakis(3',4',5'-trimethoxyphenyl)porphyrinatoiron(III) chloride

Base Information

Chemical Name:5,10,15,20-tetrakis(3',4',5'-trimethoxyphenyl)porphyrinatoiron(III) chloride
CAS No.:81245-21-8
Molecular Formula:C₅₆H₅₂ClFeN₄O₁₂
Molecular Weight:1064.35
Hs Code.:

Synonyms:5,10,15,20-tetrakis(3',4',5'-trimethoxyphenyl)porphyrinatoiron(III) chloride

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Chemical Property of 5,10,15,20-tetrakis(3',4',5'-trimethoxyphenyl)porphyrinatoiron(III) chloride

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Technology Process of 5,10,15,20-tetrakis(3',4',5'-trimethoxyphenyl)porphyrinatoiron(III) chloride

There total 1 articles about 5,10,15,20-tetrakis(3',4',5'-trimethoxyphenyl)porphyrinatoiron(III) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 109-97-7,30604-81-0
pyrrole

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: iron(II) chloride

: 81245-21-8
meso-tetrakis(3,4,5-trimethoxyphenyl)porphyriniron(III) chloride

Guidance literature:: pyrrole; 3,4,5-trimethoxy-benzaldehyde; With hydrogenchloride; In water; N,N-dimethyl-formamide; for 1h; Inert atmosphere; Schlenk technique;

iron(II) chloride; In water; N,N-dimethyl-formamide; for 8h; Schlenk technique; Reflux;
DOI:10.1002/asia.201200518

Reference yield: 90.0%

: 81245-21-8
meso-tetrakis(3,4,5-trimethoxyphenyl)porphyriniron(III) chloride

: 64-19-7,77671-22-8
acetic acid

: 7632-00-0
sodium nitrite

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: C₅₆H₅₂FeN₅O₁₃*C₂H₄O₂*C₆H₆

Guidance literature:: meso-tetrakis(3,4,5-trimethoxyphenyl)porphyriniron(III) chloride; acetic acid; sodium nitrite; benzene; for 0.166667h; Inert atmosphere; Schlenk technique;

With triphenylphosphine; for 0.583333h; Inert atmosphere; Schlenk technique;
DOI:10.1002/asia.201200518

Reference yield:

: 81245-21-8
5,10,15,20-tetrakis(3',4',5'-trimethoxyphenyl)porphyrinatoiron(III) chloride

: 83136-57-6
[meso-tetrakis(3,4,5-trimethoxyphenyl)porphyrin]iron(II)

Guidance literature:: With sodium dithionite; In dichloromethane; water; Fe-complex and sodium dithionite were dissolved in CH2Cl2 and H2O, the soln. was shaken; two layers were septd., CH2Cl2 soln. was washed with H2O, evapd., driedin vac. for 12 h, dissolved in CD2Cl2, detected by NMR (1)H;
DOI:10.1021/ja00386a027