methyl 2-((methoxycarbonyl)amino)-5-methylbenzoate

Base Information

Chemical Name:methyl 2-((methoxycarbonyl)amino)-5-methylbenzoate
CAS No.:1153421-34-1
Molecular Formula:C₁₁H₁₃NO₄
Molecular Weight:223.229
Hs Code.:

Synonyms:methyl 2-((methoxycarbonyl)amino)-5-methylbenzoate

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Chemical Property of methyl 2-((methoxycarbonyl)amino)-5-methylbenzoate

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of methyl 2-((methoxycarbonyl)amino)-5-methylbenzoate

There total 4 articles about methyl 2-((methoxycarbonyl)amino)-5-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 67-56-1
methanol

: 608-05-9
5-methyl-indole-2,3-dione

: 1153421-34-1
methyl 2-((methoxycarbonyl)amino)-5-methylbenzoate

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 3h; Electrolysis;
DOI:10.1021/acs.joc.1c01017

Reference yield: 55.0%

: 67-56-1
methanol

: 614-96-0
5-methyl-1H-indole

: 1153421-34-1
methyl 2-((methoxycarbonyl)amino)-5-methylbenzoate

Guidance literature:: With sodium nitrite; In acetonitrile; at 25 ℃; for 4h; Electrolysis;
DOI:10.1002/chem.202101527

Reference yield:

: 67-56-1
methanol

: 40314-06-5
5-methyl-1H-isoindole-1,3-(2H)-dione

: 1153421-34-1
methyl 2-((methoxycarbonyl)amino)-5-methylbenzoate

: 1356116-12-5
methyl 2-((methoxycarbonyl)amino)-4-methylbenzoate

: 18595-17-0
methyl 4-methylanthranilate

Guidance literature:: methanol; With iodobenzene; toluene-4-sulfonic acid; sodium sulfate; 3-chloro-benzenecarboperoxoic acid; at 0 ℃; for 0.166667h; Inert atmosphere;

5-methyl-1H-isoindole-1,3-(2H)-dione; With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 0 - 40 ℃; for 5h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol300028j