Technology Process of C30H46N2O12Si
There total 11 articles about C30H46N2O12Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at -78 ℃;
for 0.833333h;
chemoselective reaction;
Inert atmosphere;
DOI:10.1021/ol2021687
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C
2.1: sodium hydride / 1,4-dioxane / 60 °C / Inert atmosphere
3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere
4.1: methanol; toluene-4-sulfonic acid / 1 h / 70 °C
4.2: 20 °C
5.1: dichloromethane / 0.42 h / -78 °C / Inert atmosphere
6.1: pyridine / dichloromethane / 0.83 h / -78 °C / Inert atmosphere
With
pyridine; methanol; dmap; sodium hydride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
1,4-dioxane; dichloromethane; acetonitrile;
DOI:10.1021/ol2021687
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / 1,4-dioxane / 60 °C / Inert atmosphere
2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere
3.1: methanol; toluene-4-sulfonic acid / 1 h / 70 °C
3.2: 20 °C
4.1: dichloromethane / 0.42 h / -78 °C / Inert atmosphere
5.1: pyridine / dichloromethane / 0.83 h / -78 °C / Inert atmosphere
With
pyridine; methanol; dmap; sodium hydride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
1,4-dioxane; dichloromethane;
DOI:10.1021/ol2021687
