(E)-1-(3-(2-chlorophenyl)acryloyl)-6-iodo-1H-benzo[d][1,3]oxazine-2,4-dione

Base Information

Chemical Name:(E)-1-(3-(2-chlorophenyl)acryloyl)-6-iodo-1H-benzo[d][1,3]oxazine-2,4-dione
CAS No.:1312679-83-6
Molecular Formula:C₁₇H₉ClINO₄
Molecular Weight:453.62
Hs Code.:

Synonyms:(E)-1-(3-(2-chlorophenyl)acryloyl)-6-iodo-1H-benzo[d][1,3]oxazine-2,4-dione

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Chemical Property of (E)-1-(3-(2-chlorophenyl)acryloyl)-6-iodo-1H-benzo[d][1,3]oxazine-2,4-dione

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Technology Process of (E)-1-(3-(2-chlorophenyl)acryloyl)-6-iodo-1H-benzo[d][1,3]oxazine-2,4-dione

There total 3 articles about (E)-1-(3-(2-chlorophenyl)acryloyl)-6-iodo-1H-benzo[d][1,3]oxazine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1312679-80-3
(E)-2-(3-(2-chlorophenyl)acrylamido)-5-iodobenzoic acid

: 541-41-3
chloroformic acid ethyl ester

: 1312679-83-6
(E)-1-(3-(2-chlorophenyl)acryloyl)-6-iodo-1H-benzo[d][1,3]oxazine-2,4-dione

Guidance literature:: (E)-2-(3-(2-chlorophenyl)acrylamido)-5-iodobenzoic acid; chloroformic acid ethyl ester; for 0.25h; Reflux;

With acetyl chloride; for 0.5h; Reflux;
DOI:10.1016/j.ejmech.2011.03.067

Reference yield:

: 3752-25-8,939-58-2
o-chlorocinnamic acid

: 1312679-83-6
(E)-1-(3-(2-chlorophenyl)acryloyl)-6-iodo-1H-benzo[d][1,3]oxazine-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 5 h / Reflux

2.1: pyridine / 24 h / 0 - 5 °C

3.1: 0.25 h / Reflux

3.2: 0.5 h / Reflux

With pyridine; thionyl chloride;
DOI:10.1016/j.ejmech.2011.03.067

Reference yield:

: 5326-47-6
2-amino-5-iodobenzoic acid

: 1312679-83-6
(E)-1-(3-(2-chlorophenyl)acryloyl)-6-iodo-1H-benzo[d][1,3]oxazine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 24 h / 0 - 5 °C

2.1: 0.25 h / Reflux

2.2: 0.5 h / Reflux

With pyridine;
DOI:10.1016/j.ejmech.2011.03.067