C₁₇H₂₅F₂N₃O₂Si

Base Information

Chemical Name:C₁₇H₂₅F₂N₃O₂Si
CAS No.:1413776-17-6
Molecular Formula:C₁₇H₂₅F₂N₃O₂Si
Molecular Weight:369.487
Hs Code.:

C<sub>17</sub>H<sub>25</sub>F<sub>2</sub>N<sub>3</sub>O<sub>2</sub>Si

Synonyms:C₁₇H₂₅F₂N₃O₂Si

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Chemical Property of C₁₇H₂₅F₂N₃O₂Si

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Technology Process of C₁₇H₂₅F₂N₃O₂Si

There total 10 articles about C₁₇H₂₅F₂N₃O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394293-56-1
(S)-3-(((R)-1-amino-2-phenylethyl)diphenylsilyl)-2-methylpropanamide

: 1413776-17-6
C₁₇H₂₅F₂N₃O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-methyl-morpholine / dichloromethane; N,N-dimethyl-formamide / 14 h / -10 - 20 °C

2.1: trifluorormethanesulfonic acid / dichloromethane / 1 h / 0 °C

2.2: 0.5 h / 0 °C

3.1: hydrogen fluoride / dichloromethane / 0.17 h / pH 2 - 3

With 4-methyl-morpholine; trifluorormethanesulfonic acid; hydrogen fluoride; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol301933n

Reference yield:

: 1394293-52-7
(S)-3-(((R)-1-(1,3-dioxoisoindolin-2-yl)-2-phenylethyl)diphenylsilyl)-2-methylpropanoic acid

: 1413776-17-6
C₁₇H₂₅F₂N₃O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine; chloroformic acid ethyl ester; ammonium hydroxide / tetrahydrofuran / 2 h / -20 - -5 °C

2.1: hydrazine / ethanol / 14 h / Reflux

3.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-methyl-morpholine / dichloromethane; N,N-dimethyl-formamide / 14 h / -10 - 20 °C

4.1: trifluorormethanesulfonic acid / dichloromethane / 1 h / 0 °C

4.2: 0.5 h / 0 °C

5.1: hydrogen fluoride / dichloromethane / 0.17 h / pH 2 - 3

With 4-methyl-morpholine; ammonium hydroxide; trifluorormethanesulfonic acid; hydrogen fluoride; chloroformic acid ethyl ester; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; hydrazine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol301933n

Reference yield:

: 1394293-54-9
tert-butyl 2-((R)-1-(((S)-3-amino-2-methyl-3-oxopropyl)diphenylsilyl)-2-phenylethylcarbamoyl)pyrrolidine-1-carboxylate

: 1413776-17-6
C₁₇H₂₅F₂N₃O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluorormethanesulfonic acid / dichloromethane / 1 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: hydrogen fluoride / dichloromethane / 0.17 h / pH 2 - 3

With trifluorormethanesulfonic acid; hydrogen fluoride; In dichloromethane;
DOI:10.1021/ol301933n