[3-(4-chloro-benzylidene)-2-phenyl-cyclopentyl]-phenyl ketone

Base Information

• Chemical Name: [3-(4-chloro-benzylidene)-2-phenyl-cyclopentyl]-phenyl ketone
• CAS No.: 873962-96-0
• Molecular Formula: C₂₅H₂₁ClO
• Molecular Weight: 372.894
• Mol file: 873962-96-0.mol

Synonyms:[3-(4-chloro-benzylidene)-2-phenyl-cyclopentyl]-phenyl ketone

Chemical Property of [3-(4-chloro-benzylidene)-2-phenyl-cyclopentyl]-phenyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [3-(4-chloro-benzylidene)-2-phenyl-cyclopentyl]-phenyl ketone

There total 6 articles about [3-(4-chloro-benzylidene)-2-phenyl-cyclopentyl]-phenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chlorobenzaldehyde (104-88-1) → [3-(4-chloro-benzylidene)-2-phenyl-cyclopentyl]-phenyl ketone (873962-96-0)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol; methanol. sodium methylate / 20 °C

2: diethyl ether

With methanol; diethyl ether; sodium methylate;

DOI:10.1021/ja01274a021

Reference yield:

benzoyl chloride (98-88-4) → [3-(4-chloro-benzylidene)-2-phenyl-cyclopentyl]-phenyl ketone (873962-96-0)

Guidance literature:

Multi-step reaction with 3 steps

1: AlCl₃; carbon disulfide / -5 °C / Erhitzen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit N.N-Diaethyl-anilin auf 180grad

2: methanol; methanol. sodium methylate / 20 °C

3: diethyl ether

With methanol; carbon disulfide; aluminium trichloride; diethyl ether; sodium methylate;

DOI:10.1021/ja01274a021

Reference yield:

cyclopentene (142-29-0) → [3-(4-chloro-benzylidene)-2-phenyl-cyclopentyl]-phenyl ketone (873962-96-0)

Guidance literature:

Multi-step reaction with 3 steps

1: AlCl₃; carbon disulfide / -5 °C / Erhitzen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit N.N-Diaethyl-anilin auf 180grad

2: methanol; methanol. sodium methylate / 20 °C

3: diethyl ether

With methanol; carbon disulfide; aluminium trichloride; diethyl ether; sodium methylate;

DOI:10.1021/ja01274a021

upstream raw materials:

diethyl ether

4-chlorobenzaldehyde

benzoyl chloride

cyclopentene

Downstream raw materials:

3-benzoyl-2-phenyl-cyclopentanone

4-chlorobenzaldehyde