Technology Process of C48H71BrN2O9Si2
There total 7 articles about C48H71BrN2O9Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1016/j.tet.2015.04.064
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C
2: triethylamine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / dichloromethane / 72 h / 20 °C
3: formic acid; water / tetrahydrofuran-d8 / 10 h / 20 °C
4: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere
With
1H-imidazole; formic acid; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; triethylamine;
In
tetrahydrofuran-d8; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2015.04.064
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / dichloromethane / 72 h / 20 °C
2: formic acid; water / tetrahydrofuran-d8 / 10 h / 20 °C
3: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere
With
formic acid; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; triethylamine;
In
tetrahydrofuran-d8; dichloromethane;
DOI:10.1016/j.tet.2015.04.064
