Technology Process of 2-(2-(5-methoxy)furanyl)-3-phenyl-1-pivaloylindoline
There total 5 articles about 2-(2-(5-methoxy)furanyl)-3-phenyl-1-pivaloylindoline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride;
In
dichloromethane;
at -60 ℃;
for 0.333333h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 69 percent / manganese dioxide / ethanol; CH2Cl2 / 16 h / Ambient temperature
2: 85 percent / n-BuLi, TMEDA / hexane; tetrahydrofuran / 1.) -30 deg C, 30 min, 2.) r.t., 1 h
3: 75 percent / trifluoroacetic anhydride, dimethyl sulfoxide, triethylamine / CH2Cl2 / 0.33 h / -60 °C
With
manganese(IV) oxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride;
In
tetrahydrofuran; ethanol; hexane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium iodide / methanol
2: 61 percent / lithium aluminium hydride
3: 69 percent / manganese dioxide / ethanol; CH2Cl2 / 16 h / Ambient temperature
4: 85 percent / n-BuLi, TMEDA / hexane; tetrahydrofuran / 1.) -30 deg C, 30 min, 2.) r.t., 1 h
5: 75 percent / trifluoroacetic anhydride, dimethyl sulfoxide, triethylamine / CH2Cl2 / 0.33 h / -60 °C
With
manganese(IV) oxide; lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; sodium iodide;
In
tetrahydrofuran; methanol; ethanol; hexane; dichloromethane;