2-Methylcyclohexanone carbomethoxyhydrazone

Base Information

Chemical Name:2-Methylcyclohexanone carbomethoxyhydrazone
CAS No.:124243-23-8
Molecular Formula:C₉H₁₆N₂O₂
Molecular Weight:184.238
Hs Code.:

Synonyms:2-Methylcyclohexanone carbomethoxyhydrazone

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Chemical Property of 2-Methylcyclohexanone carbomethoxyhydrazone

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Technology Process of 2-Methylcyclohexanone carbomethoxyhydrazone

There total 1 articles about 2-Methylcyclohexanone carbomethoxyhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6294-89-9
hydrazinecarboxylic acid methyl ester

: 583-60-8
2-Methylcyclohexanone

: 124243-23-8
2-Methylcyclohexanone carbomethoxyhydrazone

Guidance literature:: With acetic acid; In methanol; for 6h; Yield given; Heating;
DOI:10.1021/jo00290a048

Reference yield: 74.0%

: 124243-23-8
2-Methylcyclohexanone carbomethoxyhydrazone

: 143-33-9,25596-52-5
sodium cyanide

: 90154-71-5
2-methylcyclohexanecarbonitrile

Guidance literature:: In methanol; at 17 ℃; for 4.7h; after standing for three days before electrolysis;
DOI:10.1021/jo00290a048

Reference yield:

: 124243-23-8
2-Methylcyclohexanone carbomethoxyhydrazone

: 90154-71-5
2-methylcyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH / methanol / Ambient temperature

2: 83 percent / NaCN / methanol / 4.7 h / 17 °C / electrolysis

With sodium cyanide; acetic acid; In methanol;
DOI:10.1021/jo00290a048