5-(2,5-dimethylphenoxy)-2,2-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

Base Information

Chemical Name:5-(2,5-dimethylphenoxy)-2,2-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide
CAS No.:1257521-31-5
Molecular Formula:C₂₂H₂₂F₇NO₂
Molecular Weight:465.411
Hs Code.:

Synonyms:5-(2,5-dimethylphenoxy)-2,2-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

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Chemical Property of 5-(2,5-dimethylphenoxy)-2,2-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

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Technology Process of 5-(2,5-dimethylphenoxy)-2,2-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

There total 2 articles about 5-(2,5-dimethylphenoxy)-2,2-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79791-29-0
2-(3-(2,5-dimethylphenoxy)propyl)-2-methylpropionyl chloride

: 651-83-2
4-trifluoromethyl-2,3,5,6-tetrafluoroaniline

: 1257521-31-5
5-(2,5-dimethylphenoxy)-2,2-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

Guidance literature:: In toluene; for 12h; Reflux;
DOI:10.1021/ja108754f

Reference yield:

: 25812-30-0
gemfibrozil

: 1257521-31-5
5-(2,5-dimethylphenoxy)-2,2-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane / 0 - 20 °C / Inert atmosphere

2: toluene / 12.5 h / 20 °C / Reflux

With oxalyl dichloride; In dichloromethane; toluene;
DOI:10.1002/anie.201502075

Reference yield: 96.0%

: 201230-82-2
carbon monoxide

: 1257521-31-5
5-(2,5-dimethylphenoxy)-2,2-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

: 1257521-51-9
3-(3-(2,5-dimethylphenoxy)propyl)-3-methyl-1-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pyrrolidine-2,5-dione

Guidance literature:: With potassium dihydrogenphosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; silver(I) acetate; palladium diacetate; In hexane; at 130 ℃; for 18h; under 760.051 Torr;
DOI:10.1021/ja108754f