5-fluoro-1,2,3-triiodobenzene

Base Information

Chemical Name:5-fluoro-1,2,3-triiodobenzene
CAS No.:1509937-21-6
Molecular Formula:C₆H₂FI₃
Molecular Weight:473.794
Hs Code.:

Synonyms:5-fluoro-1,2,3-triiodobenzene

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Chemical Property of 5-fluoro-1,2,3-triiodobenzene

Chemical Property:

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Technology Process of 5-fluoro-1,2,3-triiodobenzene

There total 3 articles about 5-fluoro-1,2,3-triiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 88162-54-3
4-fluoro-2,6-diiodoaniline

: 1509937-21-6
5-fluoro-1,2,3-triiodobenzene

Guidance literature:: 4-fluoro-2,6-diiodoaniline; With hydrogenchloride; In diethyl ether; water; at 0 ℃;

With hydrogenchloride; water; sodium nitrite; at 5 ℃; for 0.166667h;

With potassium iodide; In water; at 50 - 80 ℃;
DOI:10.1071/CH13324

Reference yield:

: 371-40-4
4-fluoroaniline

: 1509937-21-6
5-fluoro-1,2,3-triiodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; silver sulfate / ethanol / 24 h / 25 °C

2.1: hydrogenchloride / diethyl ether; water / 0 °C

2.2: 0.17 h / 5 °C

2.3: 50 - 80 °C

With hydrogenchloride; iodine; silver sulfate; In diethyl ether; ethanol; water; 2.2: |Sandmeyer Reaction / 2.3: |Sandmeyer Reaction;
DOI:10.1071/CH13324

Reference yield:

: 456-22-4
4-Fluorobenzoic acid

: 1509937-21-6
5-fluoro-1,2,3-triiodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; iodine; [bis(acetoxy)iodo]benzene / N,N-dimethyl-formamide / 24 h / 100 °C / Sealed tube

2: N-iodo-succinimide / 1,2-dichloro-ethane / 24 h / Photolysis; Reflux

With N-iodo-succinimide; [bis(acetoxy)iodo]benzene; iodine; palladium diacetate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1071/CH14386