Biphenyl-2-yl-[1-(1-methyl-1H-imidazol-2-yl)-1-phenyl-meth-(E)-ylidene]-amine

Base Information

• Chemical Name: Biphenyl-2-yl-[1-(1-methyl-1H-imidazol-2-yl)-1-phenyl-meth-(E)-ylidene]-amine
• CAS No.: 813416-08-9
• Molecular Formula: C₂₃H₁₉N₃
• Molecular Weight: 337.424

Synonyms:Biphenyl-2-yl-[1-(1-methyl-1H-imidazol-2-yl)-1-phenyl-meth-(E)-ylidene]-amine

Chemical Property of Biphenyl-2-yl-[1-(1-methyl-1H-imidazol-2-yl)-1-phenyl-meth-(E)-ylidene]-amine

Chemical Property:

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Technology Process of Biphenyl-2-yl-[1-(1-methyl-1H-imidazol-2-yl)-1-phenyl-meth-(E)-ylidene]-amine

There total 2 articles about Biphenyl-2-yl-[1-(1-methyl-1H-imidazol-2-yl)-1-phenyl-meth-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-phenylaniline (90-41-5) + (1-methyl-1H-imidazol-2-yl)(phenyl)methanone (30148-17-5) → Biphenyl-2-yl-[1-(1-methyl-1H-imidazol-2-yl)-1-phenyl-meth-(E)-ylidene]-amine (813416-08-9)

Guidance literature:

2-phenylaniline; With trimethylaluminum; In toluene; at 80 ℃; for 1.5h;

(1-methyl-1H-imidazol-2-yl)(phenyl)methanone; In toluene; at 20 ℃; for 48h;

DOI:10.1002/ejic.200400070

Reference yield:

benzoyl chloride (98-88-4) → Biphenyl-2-yl-[1-(1-methyl-1H-imidazol-2-yl)-1-phenyl-meth-(E)-ylidene]-amine (813416-08-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 75 percent / Et₃N / acetonitrile / 20 °C

2.1: Me₃Al / toluene / 1.5 h / 80 °C

2.2: 85 percent / toluene / 48 h / 20 °C

With trimethylaluminum; triethylamine; In toluene; acetonitrile;

DOI:10.1002/ejic.200400070

Reference yield: 99.0%

nickel(II) bromide dimethoxyethane + Biphenyl-2-yl-[1-(1-methyl-1H-imidazol-2-yl)-1-phenyl-meth-(E)-ylidene]-amine (813416-08-9) → 2Br(1-)*Ni(2+)*C6H5C6H4NC(C6H5)C3H2N2(CH3)=[Br2Ni(C6H5C6H4NC(C6H5)C3H2N2(CH3))]

Guidance literature:

In dichloromethane; stirred at room temp. for 48 h; solvent removed (vac.); elem. anal.;

DOI:10.1002/ejic.200400070

upstream raw materials:

2-phenylaniline

(1-methyl-1H-imidazol-2-yl)(phenyl)methanone

benzoyl chloride

Downstream raw materials:

[Cl₂Pd(C₆H₅C₆H₄NC(C₆H₅)C₃H₂N₂(CH₃))]

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