(+)-(3R,4S)-cis-4-[(S)-2,2-dimethyl-1,3-dioxolane-4-yl]-1(2-propynyl)-3-phenoxy-2-azetidinone

Base Information

Chemical Name:(+)-(3R,4S)-cis-4-[(S)-2,2-dimethyl-1,3-dioxolane-4-yl]-1(2-propynyl)-3-phenoxy-2-azetidinone
CAS No.:164354-45-4
Molecular Formula:C₁₇H₁₉NO₄
Molecular Weight:301.342
Hs Code.:

Synonyms:(+)-(3R,4S)-cis-4-[(S)-2,2-dimethyl-1,3-dioxolane-4-yl]-1(2-propynyl)-3-phenoxy-2-azetidinone

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Chemical Property of (+)-(3R,4S)-cis-4-[(S)-2,2-dimethyl-1,3-dioxolane-4-yl]-1(2-propynyl)-3-phenoxy-2-azetidinone

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Technology Process of (+)-(3R,4S)-cis-4-[(S)-2,2-dimethyl-1,3-dioxolane-4-yl]-1(2-propynyl)-3-phenoxy-2-azetidinone

There total 2 articles about (+)-(3R,4S)-cis-4-[(S)-2,2-dimethyl-1,3-dioxolane-4-yl]-1(2-propynyl)-3-phenoxy-2-azetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 701-99-5
Phenoxyacetyl chloride

: [1-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-meth-(E)-ylidene]-prop-2-ynyl-amine

: 164354-45-4
(+)-(3R,4S)-cis-4-[(S)-2,2-dimethyl-1,3-dioxolane-4-yl]-1(2-propynyl)-3-phenoxy-2-azetidinone

Guidance literature:: With triethylamine; In benzene; Ambient temperature;
DOI:10.1021/jo980114h

Reference yield:

: 701-99-5
Phenoxyacetyl chloride

: 214477-36-8
[1-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-meth-(E)-ylidene]-prop-2-ynyl-amine

: 164354-45-4
(+)-(3R,4S)-cis-4-[(S)-2,2-dimethyl-1,3-dioxolane-4-yl]-1(2-propynyl)-3-phenoxy-2-azetidinone

Guidance literature:: With triethylamine;
DOI:10.1021/jo9823994

Reference yield: 87.0%

: 164354-45-4
(+)-(3R,4S)-cis-4-[(S)-2,2-dimethyl-1,3-dioxolane-4-yl]-1(2-propynyl)-3-phenoxy-2-azetidinone

: 251480-02-1
(+)-(3R,4R)-cis-4-formyl-3-phenoxy-1-(2-propynyl)-2-azetidinone

Guidance literature:: (+)-(3R,4S)-cis-4-[(S)-2,2-dimethyl-1,3-dioxolane-4-yl]-1(2-propynyl)-3-phenoxy-2-azetidinone; With toluene-4-sulfonic acid; In tetrahydrofuran; water; Heating;

With sodium periodate; sodium hydrogencarbonate; In dichloromethane; water; Further stages.;
DOI:10.1021/jo991984h