allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside
CAS No.:128745-41-5
Molecular Formula:C₂₄H₂₇NO₇
Molecular Weight:441.481
Hs Code.:

Synonyms:allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

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Chemical Property of allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

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Technology Process of allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

There total 1 articles about allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 83663-03-0
benzyl ((2S,3R,4R,5S,6R)-2-(allyloxy)-4,5-dihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-3-yl)carbamate

: 100-52-7
benzaldehyde

: 128745-41-5
allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Guidance literature:: With zinc(II) chloride; for 16h; Ambient temperature;
DOI:10.1016/0008-6215(89)85012-8

Reference yield: 97.0%

: 128745-41-5
allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

: 128745-42-6
allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-ribo-hexapyranosid-3-ulose

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃; for 1.5h;
DOI:10.1016/0008-6215(89)85012-8

Reference yield:

: 128745-41-5
allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

: 128745-43-7
allyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / DMSO, oxalyl chloride, Et₃N / CH₂Cl₂ / 1.5 h / -78 °C

2: 85.4 percent / sodium borohydride / dimethylformamide; methanol / 2 h / 0 °C

With sodium tetrahydroborate; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(89)85012-8