Technology Process of C32H35N3O5
There total 9 articles about C32H35N3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C8H17N3*2ClH; C24H22O7;
With
sodium acetate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 1h;
Inert atmosphere;
With
acetic acid;
In
N,N-dimethyl-formamide;
at 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: water; toluene; methanol / 20 °C / Inert atmosphere
2.1: hydrogenchloride; sodium cyanoborohydride / water; methanol / 1.5 h / 20 °C / pH 4 / Inert atmosphere; Cooling with ice
3.1: methanol; hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere
4.1: sodium acetate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
4.2: 20 °C / Inert atmosphere
With
hydrogenchloride; methanol; sodium acetate; sodium cyanoborohydride;
In
1,4-dioxane; methanol; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; sodium cyanoborohydride / water; methanol / 1.5 h / 20 °C / pH 4 / Inert atmosphere; Cooling with ice
2.1: methanol; hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere
3.1: sodium acetate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
With
hydrogenchloride; methanol; sodium acetate; sodium cyanoborohydride;
In
1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
