3-(3-bromo-4-iodophenyl)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole

Base Information

Chemical Name:3-(3-bromo-4-iodophenyl)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole
CAS No.:1357614-71-1
Molecular Formula:C₁₆H₇BrCl₃F₃INO
Molecular Weight:599.4
Hs Code.:

Synonyms:3-(3-bromo-4-iodophenyl)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole

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Chemical Property of 3-(3-bromo-4-iodophenyl)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole

Chemical Property:

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Technology Process of 3-(3-bromo-4-iodophenyl)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole

There total 6 articles about 3-(3-bromo-4-iodophenyl)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 864736-87-8
1,2,3-trichloro-5-(1,1,1-trifluoroprop-2-en-2-yl)benzene

: 1357614-72-2
C₇H₄BrClINO

: 1357614-71-1
3-(3-bromo-4-iodophenyl)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole

Guidance literature:: With potassium hydrogencarbonate; In ethyl acetate; at 20 ℃;

Reference yield:

: 249647-24-3
3-bromo-4-iodobenzoic acid methyl ester

: 1357614-71-1
3-(3-bromo-4-iodophenyl)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / dichloromethane / -78 - 20 °C / Inert atmosphere

1.2: 0.5 h / 20 °C

2.1: sodium hydrogencarbonate; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / water; dichloromethane / 0 - 20 °C

3.1: hydroxylamine hydrochloride / water; ethanol / 19 h / 20 - 50 °C

4.1: N-chloro-succinimide / N,N-dimethyl-formamide / 18 h / 20 °C

5.1: potassium hydrogencarbonate / ethyl acetate / 20 °C

With sodium hypochlorite; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydroxylamine hydrochloride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium hydrogencarbonate; sodium bromide; In ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 249647-26-5
(3-bromo-4-iodophenyl)methanol

: 1357614-71-1
3-(3-bromo-4-iodophenyl)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / water; dichloromethane / 0 - 20 °C

2: hydroxylamine hydrochloride / water; ethanol / 19 h / 20 - 50 °C

3: N-chloro-succinimide / N,N-dimethyl-formamide / 18 h / 20 °C

4: potassium hydrogencarbonate / ethyl acetate / 20 °C

With sodium hypochlorite; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydroxylamine hydrochloride; sodium hydrogencarbonate; potassium hydrogencarbonate; sodium bromide; In ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;