(+/-)-[4-(7-chloro-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl)-3-methylpiperazin-1-yl]phenylmethanone

Base Information

Chemical Name:(+/-)-[4-(7-chloro-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl)-3-methylpiperazin-1-yl]phenylmethanone
CAS No.:1001411-95-5
Molecular Formula:C₁₉H₁₉ClN₄O₃S
Molecular Weight:418.904
Hs Code.:

Synonyms:(+/-)-[4-(7-chloro-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl)-3-methylpiperazin-1-yl]phenylmethanone

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Chemical Property of (+/-)-[4-(7-chloro-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl)-3-methylpiperazin-1-yl]phenylmethanone

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Technology Process of (+/-)-[4-(7-chloro-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl)-3-methylpiperazin-1-yl]phenylmethanone

There total 1 articles about (+/-)-[4-(7-chloro-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl)-3-methylpiperazin-1-yl]phenylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1001413-18-8
7-chloro-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl chloride

: 75349-23-4
(+/-)-(3-methylpiperazin-1-yl)phenylmethanone

: 1001411-95-5
(+/-)-[4-(7-chloro-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl)-3-methylpiperazin-1-yl]phenylmethanone

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; Heating;
DOI:10.1021/jm070650e

Reference yield: 71.0%

: 557-21-1
zinc(II) cyanide

: 1001411-95-5
(+/-)-[4-(7-chloro-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl)-3-methylpiperazin-1-yl]phenylmethanone

: 1001412-95-8
3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridine-7-carbonitrile

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; zinc; In N,N-dimethyl acetamide; at 130 ℃; for 1h; microwave irradiation;
DOI:10.1021/jm070650e

Reference yield: 31.0%

: 1001411-95-5
(+/-)-[4-(7-chloro-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl)-3-methylpiperazin-1-yl]phenylmethanone

: 121359-48-6
2-(tri-n-butylstannyl)thiazole

: 1001412-25-4
[3-methyl-4-(7-thiazol-2-yl-1H-pyrrolo[2,3-c]pyridine-3-sulfonyl)-piperazin-1-yl]phenylmethanone

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 150 ℃; for 0.333333h; microwave irradiation;
DOI:10.1021/jm070650e