13-(phenylthio)isoalantolactone

Base Information

Chemical Name:13-(phenylthio)isoalantolactone
CAS No.:69993-35-7
Molecular Formula:C₂₁H₂₆O₂S
Molecular Weight:342.502
Hs Code.:

Synonyms:13-(phenylthio)isoalantolactone

Suppliers and Price of 13-(phenylthio)isoalantolactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 13-(phenylthio)isoalantolactone

Chemical Property:

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Technology Process of 13-(phenylthio)isoalantolactone

There total 3 articles about 13-(phenylthio)isoalantolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 470-17-7
isoalantolactone

: 930-69-8
sodium thiophenolate

: 69993-35-7
13-(phenylthio)isoalantolactone

Guidance literature:: In ethanol; for 2h; Ambient temperature;
DOI:10.1021/jo00287a024

Reference yield:

: 123489-82-7
11β-phenylseleno-5,7,8αH-eudesm-4(15)-en-8,12-olide

: 69993-35-7
13-(phenylthio)isoalantolactone

Guidance literature:: Multi-step reaction with 2 steps

1: 30 mg / aq. H₂O₂ / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 95 percent / ethanol / 2 h / Ambient temperature

With dihydrogen peroxide; In ethanol; dichloromethane;
DOI:10.1021/jo00287a024

Reference yield:

: 1856-58-2
11,13-dihydroisoalantolactone

: 69993-35-7
13-(phenylthio)isoalantolactone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium isopropylcyclohexylamine / 1.) hexane, THF, -78 deg C, 1 h, 2.) hexane, THF, from -78 deg C to -20 deg C

2: 30 mg / aq. H₂O₂ / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 95 percent / ethanol / 2 h / Ambient temperature

With dihydrogen peroxide; lithium cyclohexylisopropylamide; In ethanol; dichloromethane;
DOI:10.1021/jo00287a024