Technology Process of C38H40F4N6O4
There total 4 articles about C38H40F4N6O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium acetate;
In
xylene;
at 140 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
2: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C
3: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 3 h / 20 °C
4: ammonium acetate / xylene / 4 h / 140 °C / Sealed tube
With
hydrogenchloride; ammonium acetate; N-ethyl-N,N-diisopropylamine; HATU;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; N,N-dimethyl-formamide; xylene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydrogencarbonate / dichloromethane / 20 °C
1.2: 2 h / 20 °C
2.1: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
3.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 3 h / 20 °C
5.1: ammonium acetate / xylene / 4 h / 140 °C / Sealed tube
With
hydrogenchloride; ammonium acetate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; HATU;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; xylene;
